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[Anonymous], FUTURE DIRECTIONS Important next steps to build on the findings presented here include further use of cross-technique comparisons for the exploration of smectite hydration. Repetition of techniques such as TGA-MS and 23Na NMR alongside RH-controlled XRD with additional swelling clays and alternate cation loadings would be insightful. Further probing of organic structures adsorbed to smectite clays including the introduction of unique functional groups and direct stereochemistry inv
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