Crystal structure of bis(μ2-5-nonanoylquinolin-8-olato)bis[aquadichloridoindium(III)]

被引：0
|
作者：
Fuhrmann, Betty [1 ]
Meier, Eric [1 ]
Mazik, Monika [1 ]
机构：
[1] Tech Univ Bergakad Freibe, Leipziger Str 29, D-09596 Freiberg, Germany
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2024年 / 80卷
关键词：
crystal structure; indium complex; quinoline; 8-hydroxyquinoline; hydrogen bonds; van der Waals interactions; ALUMINUM METAL-COMPLEX; SOLVENT-EXTRACTION; 8-HYDROXYQUINOLINES; GALLIUM(III); PHOTOPHYSICS;
D O I：
10.1107/S205698902400882X
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
Crystallization of 5-nonanoyl-8-hydroxyquinoline in the presence of InCl3 in acetonitrile yields a dinuclear In-III complex crystallizing in the space group P (1) over bar. In this complex, [In-2(C18H22NO2)(2)Cl-4(H2O)(2)], each indium ion is sixfold coordinated by two chloride ions, one water molecule and two 8-quinolinolate ions. The crystal of the title complex is composed of two-dimensional supramolecular aggregates, resulting from the linkage of the O-water-H center dot center dot center dot O=C and O-water-H center dot center dot center dot Cl hydrogen bonds as well as bifurcated C-arene-H center dot center dot center dot Cl contacts.
引用
收藏
页码：1020 / +
页数：10
相关论文
共 50 条
  • [1] Bis(triphenylphosphine)iminium bis(methoxo)phthalocyaninato(2)ferrate(III) - Synthesis and crystal structure
    Potz, R
    Huckstadt, H
    Homborg, H
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1998, 624 (02): : 173 - 174
  • [2] Crystal structure of 2,3-bis(2-pyridyl)-5, 8-dimethoxyquinoxaline
    He Liu
    Bo-Hua Zhong
    Li-Ping Liu
    Shi-Tian Han
    Journal of Chemical Crystallography, 2004, 34 : 265 - 268
  • [3] Crystal structure of 2,3-bis(2-pyridyl)-5, 8-dimethoxyquinoxaline
    Liu, H
    Zhong, BH
    Liu, LP
    Han, ST
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2004, 34 (04) : 265 - 268
  • [4] Crystal structure and Hirshfeld surface analysis of bis(μ-4-tert-butoxy-4-oxobut-2-en-2-olato)bis[(4-tert-butoxy-4-oxobut-2-en-2-olato)ethanolzinc(II)]
    Shtokvysh, Olherd O.
    Dyakonenko, Viktoriya V.
    Koval, Lyudmila I.
    Pekhnyo, Vasyl I.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2023, 79 : 478 - +
  • [5] Crystal structure of bis[4-(dimethylamino)pyridinium] bis(2-nitrobenzoate) trihydrate
    Sivakumar, N.
    Muralidharan, S.
    Chakkaravarthi, G.
    Velmurugan, D.
    Anbalagan, G.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 221 - +
  • [6] Synthesis and crystal structure of bis(p-aminotoluene)-bis(dimethylglyoximato) cobalt(III) perchlorate
    Chen, LJ
    Lin, S
    Yang, MX
    Liu, SX
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2003, 22 (03) : 255 - 259
  • [7] Crystal structure of bis(2-aminoanilinium) hydrogen phosphate
    Ittyachan, Reena
    Ahigna, Melesuparambil Sundaram
    Jagan, Rajamony
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2016, 72 : 530 - +
  • [8] Crystal structure of tetraethylammonium di-μ2-sulfido-bis[dibromoiron(III)]
    Deng, YH
    Wen, TB
    Zhu, HP
    Chen, CN
    Liu, QT
    ACTA CHIMICA SINICA, 1999, 57 (08) : 846 - 851
  • [9] Crystal structure of bis(μ2-triphenylacetato-κO:κO′)bis(diisobutylaluminium)
    Vinogradov, Alexander A.
    Minyaev, Mikhail E.
    Lyssenko, Konstantin A.
    Nifant'ev, Ilya E.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2019, 75 : 456 - +
  • [10] Synthesis and crystal structures of bis[1-oxopyridin-2-olato(1-)]bis(pentafluorophenyl)silicon(IV)-tetrahydrofuran-pentane (2/1/1), bis[1-oxopyridin-2-olato(1-)]bis(p-tolyl)silicon(IV), and dimesitylbis[1-oxopyridin-2-olato(1-)]silicon(IV)
    Kraft, Bradley M.
    Brennessel, William W.
    Andrews, Jordan W.
    Viggiani, Michael T.
    Kittrell, Nathan F.
    Heckman, Matthew T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2024, 80 : 318 - +
12345