The integration of Raman spectrometer with glove box for high-purity investigation in an inert gas condition

被引：0

作者：

Piskorski, Michal ^{[1
]}

Lutsyk, Iaroslav ^{[1
]}

Rys, Wojciech ^{[1
]}

Le Ster, Maxime ^{[1
]}

Ogorzalek-Sory, Zuzanna ^{[2
]}

Binder, Johannes ^{[2
]}

Toczek, Klaudia ^{[1
]}

Nadolska, Aleksandra ^{[1
]}

Dunal, Rafal ^{[1
]}

Przybysz, Przemyslaw ^{[1
]}

Rogala, Maciej ^{[1
]}

Dabrowski, Pawel ^{[1
]}

Pacuski, Wojciech ^{[2
]}

Sadowski, Janusz ^{[2
,3
,4
]}

Gryglas-Borysiewicz, Marta ^{[2
]}

Wysmolek, Andrzej ^{[2
]}

Kowalczyk, Pawel J. ^{[1
]}

Kozlowski, Witold ^{[1
]}

Krukowski, Pawel ^{[1
]}

机构：

[1] Univ Lodz, Fac Phys & Appl Informat, Pomorska 149-153, Lodz, Poland

[2] Univ Warsaw, Fac Phys, Pasteura 5, Warsaw, Poland

[3] Polish Acad Sci, Inst Phys, Aleja Lotnikow 32-46, Warsaw, Poland

[4] Ensemble3 Ctr Excellence, Wolczynska 133, Warsaw, Poland

来源：

MEASUREMENT | 2025年 / 251卷

关键词：

Raman spectroscopy; Glove box; Reactive materials; Dirhenium heptoxide; Molybdenum ditelluride; SPECTROSCOPY; SURFACE; OXIDE; OXIDATION; LIQUID; PASSIVATION; SCATTERING; MOLECULES; OXO;

D O I：

10.1016/j.measurement.2025.117190

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

We present our integration of a Raman spectrometer with a glove box, which opens the possibility to conduct studies in a high-purity inert gas conditions. This innovative setup allows for the fabrication, optical inspection, and characterization of reactive materials under strictly controlled conditions, ensuring seamless operation without exposing samples to the external environment and thus significantly enhancing research reliability. Our development work included designing a system for point, line, and mapping analysis. The open architecture allows easy modifications and the addition of new components, synchronized via software or electronics. As a proof of concept, we show results recorded on Re2O7 powder and ultrathin films of 2H-MoTe2 grown on GaAs (111)B, which are highly unstable in air and provide clear evidence that sample stability is maintained, allowing in-depth, long-lasting investigations. This research validates the key advantages of our solution in real-world applications.

引用

页数：9

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