Efficient extraction and detection of cinnamaldehyde and cinnamic acid in cinnamon twig

被引:0
作者
Zhou, Zhen [1 ,2 ]
Liu, Shengkai [1 ,2 ,3 ,4 ]
Cui, Liying [1 ,2 ,3 ,4 ]
Liu, Zhongkai [1 ,2 ,3 ,4 ]
Li, Xiaoyu [1 ,2 ,3 ,4 ]
Liu, Zhiguo [1 ,2 ,3 ,4 ]
Fu, Yujie [1 ,3 ]
机构
[1] Northeast Forestry Univ, Key Lab Forest Plant Ecol, Minist Educ, Harbin 150040, Peoples R China
[2] Northeast Forestry Univ, Coll Chem Chem Engn & Resource Utilizat, Harbin 150040, Peoples R China
[3] Northeast Forestry Univ, Engn Res Ctr Forest Biopreparat, Minist Educ, Harbin 150040, Peoples R China
[4] Northeast Forestry Univ, Heilongjiang Prov Key Lab Ecol Utilizat Forestry B, Harbin 150040, Peoples R China
关键词
Cinnamaldehyde; Cinnamic acid; Ultrasonic-microwave extraction method; HPLC; MICROWAVE-ASSISTED EXTRACTION; CASSIA; BARK; OPTIMIZATION;
D O I
10.1007/s11694-024-02994-w
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
This study explored the ultrasonic-microwave synergistic extraction technique for obtaining cinnamaldehyde and cinnamic acid from cinnamon twigs, and determined the most favorable extraction conditions. The optimization of extraction parameters, including extraction time, ethanol concentration, liquid-to-solid ratio, and microwave power, was achieved through single-factor experiments and the response surface method. The results of the significance analysis indicated that ethanol concentration and extraction power were the two primary factors affecting the extraction rates of cinnamaldehyde and cinnamic acid. Under the optimal conditions-600 W microwave power, 75% ethanol concentration, a liquid-to-solid ratio of 1:15, and a 20-min extraction time--the extraction efficiency of cinnamaldehyde and cinnamic acid was significantly improved compared to traditional methods. Moreover, the use of the ultrasonic-microwave synergistic extraction technique demonstrated higher efficiency and lower environmental impact due to reduced waste production. The study also revealed that cinnamaldehyde and cinnamic acid in cinnamon twigs exhibited strong polarity characteristics and microwave absorption capacity, contributing to enhanced cell disruption and increased natural product release. These findings provide a robust basis for the development of an efficient and environmentally friendly extraction process for these valuable bioactive compounds.
引用
收藏
页码:619 / 629
页数:11
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