Improving strength-ductility of Mg-8.5Gd-4.5Y-0.8Zn-0.4Zr magnesium alloy due to bimodal LPSO and <c + a> dislocations

被引:0
作者
Zhang, Xiaohua [1 ]
Shi, Yuan [1 ]
Li, Jiaqi [1 ]
Yue, Hongyan [1 ]
Li, Chao [1 ]
Guo, Siming [2 ]
Chen, Qiang [3 ]
机构
[1] Harbin Univ Sci & Technol, Sch Mat Sci & Chem Engn, Harbin 150040, Peoples R China
[2] Binary Univ Management & Entrepreneurship, Sch Binary Grad, Puchong 47100, Malaysia
[3] Southwest Technol & Engn Res Inst, Chongqing 400039, Peoples R China
关键词
Rare earths; Magnesium alloy; Solution treatment; LPSO; Texture; Mechanical properties; ZN-ZR ALLOY; STACKING ORDERED PHASE; MECHANICAL-PROPERTIES; MG-GD; DYNAMIC RECRYSTALLIZATION; Y-ALLOY; HOT COMPRESSION; MICROSTRUCTURE; BEHAVIOR; TRANSFORMATION;
D O I
10.1016/j.jre.2024.03.010
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
Rare-earth (RE) magnesium alloys have attracted lots of attention due to their excellent mechanical properties. In this work, the microstructure and mechanical properties of as-extruded 8.5Gd-4.5Y-0.8Zn-0.4Zr magnesium alloy under different solution treatment were examined with the optical microscope (OM), scanning electron microscope (SEM), high resolution transmission electron microscope (HRTEM), electron back-scattered diffraction (EBSD) and Instron testing machine. The results show that the ES12 alloy (solution treatment for 12 h at 520 degrees C) has the highest ultimate tensile strength (UTS) of 390 MPa with a fracture elongation of 24.5% at the cost of a minor drop in yielding strength (YS) compared to the as-extruded alloy. During solution treatment, the block-shaped long period stacking ordered (LPSO) in as-extruded alloy evolves into plate-shaped LPSO, which disperses at grain boundaries (GBs), and lamellar LPSO, which distributes in grains. The coexistence of plate-shaped and lamellar LPSO, which impedes the dislocations movement, and the activated <c + a> dislocations are regarded as the primary reasons for mechanical properties improvement. Furthermore, the (11-21) <1-100> texture in as-extruded alloy transforms into the (11-20) <0001> texture in ES12 alloy. The average grain size increases from 3.45 mu m in as-extruded alloy to 18.70 mu m in ES12 alloy. The Schmid factors of {0001} <11-20>, {10-10} <11-20>, {10-11} <11-20>, and {11-22} <11-23> increase, which indicate that slip systems are more easily activated in plastic deformation. The dynamic recrystallization (DRX) grains fraction increase to 92.8% for ES12 alloy due to the particle-stimulated nucleation (PSN) mechanism triggered by block-shaped and plate-shaped LPSO. The freshly DRXed grains further weaken the texture, and reduce the dislocation density. All of these factors increase elongation of RE magnesium alloy. (c) 2024 Chinese Society of Rare Earths. Published by Elsevier B.V. All rights are reserved, including those for text and data mining, AI training, and similar technologies.
引用
收藏
页码:832 / 842
页数:11
相关论文
共 73 条
  • [21] Microstructure and strengthening mechanism of high strength Mg-10Gd-2Y-0.5Zr alloy
    He, S. M.
    Zeng, X. Q.
    Peng, L. M.
    Gao, X.
    Nie, J. F.
    Ding, W. J.
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2007, 427 (1-2) : 316 - 323
  • [22] Humphreys FJ., 2004, Recrystallization and related annealing phenomena, DOI DOI 10.1016/B978-0-08-044164-1.X5000-2
  • [23] Anomalous effects of strain rate on the room-temperature ductility of a cast Mg-Gd-Y-Zr alloy
    Li, J. L.
    Wu, D.
    Chen, R. S.
    Han, E. H.
    [J]. ACTA MATERIALIA, 2018, 159 : 31 - 45
  • [24] The contribution of long-period stacking-ordered structure (LPSO) to high strength-high ductility combination and nanoscale deformation behavior of magnesium-rare earth alloy
    Li, K.
    Injeti, V. S. Y.
    Misra, R. D. K.
    Meng, L. G.
    Zhang, X. G.
    [J]. MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2018, 713 : 112 - 117
  • [25] Development of high-strength magnesium alloys via combined processes of extrusion, rolling and ageing
    Li, R. G.
    Nie, J. F.
    Huang, G. J.
    Xin, Y. C.
    Liu, Q.
    [J]. SCRIPTA MATERIALIA, 2011, 64 (10) : 950 - 953
  • [26] Effect of long-period stacking ordered phase on thermal stability of refined grains in Mg-RE-based alloys
    Li, Y. X.
    Qiu, D.
    Rong, Y. H.
    Zhang, M. X.
    [J]. PHILOSOPHICAL MAGAZINE, 2014, 94 (12) : 1311 - 1326
  • [27] Recent research and advances in extrusion forming of magnesium alloys: A review
    Li, Yuan Qi
    Li, Feng
    Kang, Fu Wei
    Du, Hua Qiu
    Chen, Zi Yu
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2023, 953
  • [28] A two-step dynamic recrystallization induced by LPSO phases and its impact on mechanical property of severe plastic deformation processed Mg97Y2Zn1 alloy
    Liu, Huan
    Ju, Jia
    Yang, Xiaowei
    Yan, Jingli
    Song, Dan
    Jiang, Jinghua
    Ma, Aibin
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2017, 704 : 509 - 517
  • [29] Role of the LPSO structure in the improvement of corrosion resistance of Mg-Gd-Zn-Zr alloys
    Liu, Jing
    Yang, Lixin
    Zhang, Chunyan
    Zhang, Bo
    Zhang, Tao
    Li, Yang
    Wu, Kaiming
    Wang, Fuhui
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2019, 782 : 648 - 658
  • [30] Effect of ageing treatment on the microstructures and mechanical properties of the extruded Mg-7Y-4Gd-1.5Zn-0.4Zr alloy
    Liu, Ke
    Rokhlin, L. L.
    Elkin, F. M.
    Tang, Dingxiang
    Meng, Jian
    [J]. MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2010, 527 (03): : 828 - 834