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[Anonymous], In summary, we have studied the use of a one-step hydrothermal synthesis to develop self-supported electrodes for LIB applications. We observe that the material exhibits three energy storage mechanisms: first, the conversion of MoS2 and MoOx to Mo metal, LixMoyOz, and Li2S
[9]
second, the oxidation of Mo to MoO3 and partial delithiation of LixMoyOz
[10]
and third, the formation/reduction of polysulfides. The dominant, reversible reaction is the conversion between Mo and MoO3. The unique petaled structure and large, intermediate, MoSxOy layer provide high surface area and O to support the Mo-MoO3 and Li2S-Sn2- conversion reactions. The material exhibits a maximum capacity of 3.8 mAh/cm3 (~825 mAh/g). Isolating the polysulfide formation/reduction mechanism by cycling from 1.5 - 3.0 V results in a high voltage capacity of 0.42 mAh/cm3 (350 mAh/g