Effect of Severe Plastic Deformation on the Structure and State of Grain Boundaries in Niobium

被引:0
作者
Popov, V. V. [1 ]
Popova, E. N. [1 ]
Osinnikov, E. V. [1 ]
机构
[1] RAS, MN Miheev Inst Met Phys, Ural Branch, Ekaterinburg 620108, Russia
关键词
Niobium; Severe plastic deformation; High-pressure torsion; Grain boundaries; Microhardness; Scanning tunneling microscopy; HIGH-PRESSURE TORSION; THERMAL-STABILITY; NB; EVOLUTION; DIFFUSION; ENERGY; TEMPERATURE; NICKEL; ALLOYS; MICROSTRUCTURE;
D O I
10.1007/s12540-024-01871-x
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The effect of severe plastic deformation by high-pressure torsion (HPT) on the formation of nanocrystalline structure in niobium has been studied by the methods of transmission electron microscopy, scanning tunneling microscopy, X-ray diffraction analysis and microhardness measurements. The thermal stability of the resulting structure has been analyzed. Specific features of grain boundaries (GBs) formed under the severe plastic deformation have been considered and analyzed. It is demonstrated that a considerable fraction of these boundaries are in the so-called nonequilibrium, or deformation-modified state, characterized by higher free energy and larger free volume in comparison with those of common relaxed GBs. It has been shown that contribution of nonequilibrium GBs to total strengthening is relatively small.
引用
收藏
页码:2069 / 2081
页数:13
相关论文
共 60 条
[1]   A scanning force microscopy study of grain boundary energy in copper subjected to equal channel angular pressing [J].
Amouyal, Y. ;
Rabkin, E. .
ACTA MATERIALIA, 2007, 55 (20) :6681-6689
[2]   Correlation between grain boundary energy and geometry in Ni-rich NiAl [J].
Amouyal, Y ;
Rabkin, E ;
Mishin, Y .
ACTA MATERIALIA, 2005, 53 (14) :3795-3805
[3]  
[Anonymous], 2013, NIOBIUM CHEM PROPERT
[4]  
Camilo CC., 2011, BRAZ J BIOM ENG, V27, P175, DOI [10.4322/rbeb.2011.014, DOI 10.4322/RBEB.2011.014]
[5]   Purification of Niobium by Multiple Electron Beam Melting for Superconducting RF Cavities [J].
Choi, Good-Sun ;
Lim, Jae-Won ;
Munirathnam, N. R. ;
Kim, Il-Ho .
METALS AND MATERIALS INTERNATIONAL, 2009, 15 (03) :385-390
[6]   Influence of the relaxation processes on the structure formation in pure metals and alloys under high-pressure torsion [J].
Degtyarev, M. V. ;
Chashchukhina, T. I. ;
Voronova, L. M. ;
Patselov, A. M. ;
Pilyugin, V. P. .
ACTA MATERIALIA, 2007, 55 (18) :6039-6050
[7]   Recrystallization of submicrocrystalline niobium upon heating above and below the temperature of thermally activated nucleation [J].
Degtyarev, M. V. ;
Voronova, L. M. ;
Chashchukhina, T. I. ;
Shinyavskii, D. V. ;
Levit, V. I. .
PHYSICS OF METALS AND METALLOGRAPHY, 2016, 117 (11) :1111-1118
[8]   Microstructure and texture evolution of Cu-Nb composite wires [J].
Deng, Liping ;
Yang, Xiaofang ;
Han, Ke ;
Lu, Yafeng ;
Liang, Ming ;
Liu, Qing .
MATERIALS CHARACTERIZATION, 2013, 81 :124-133
[9]   Structure and Properties of High-Strength Cu-7.7Nb Composite Wires under Various Steps of Strain and Annealing Modes [J].
Deryagina, Irina L. ;
Popova, Elena N. ;
Patrakov, Evgeny I. .
METALS, 2023, 13 (09)
[10]   Ultra-fast diffusion channels in pure Ni severely deformed by equal-channel angular pressing [J].
Divinski, Sergiy V. ;
Reglitz, Gerrit ;
Roesner, Harald ;
Estrin, Yuri ;
Wilde, Gerhard .
ACTA MATERIALIA, 2011, 59 (05) :1974-1985