Crystal structure and Hirshfeld surface analysis of 1-[6-bromo-2-(4-fluorophenyl)-1,2,3,4-tetrahydroquinolin-4-yl]pyrrolidin-2-one

被引：1

作者：

Pronina, Anastasia A. ^{[1
]}

Podrezova, Alexandra G. ^{[1
]}

Grigoriev, Mikhail S. ^{[2
]}

Hasanov, Khudayar I. ^{[3
,4
]}

Sadikhova, Nurlana D. ^{[5
]}

Akkurt, Mehmet ^{[6
]}

Bhattarai, Ajaya ^{[7
]}

机构：

[1] RUDN Univ, 6 Miklukho Maklaya St, Moscow 117198, Russia

[2] Russian Acad Sci, Frumkin Inst Phys Chem & Electrochem, Leninskiy prospect 31-4, Moscow 119071, Russia

[3] Western Caspian Univ, Istiqlaliyyat St 31, AZ-1001 Baku, Azerbaijan

[4] Azerbaijan Med Univ, Sci Res Ctr SRC, A Kasumzade St 14, AZ-1022 Baku, Azerbaijan

[5] Baku State Univ, Dept Chem, Z Xalilov Str, AZ-1148 Baku, Azerbaijan

[6] Erciyes Univ, Dept Phys, Fac Sci, TR-38039 Kayseri, Turkiye

[7] MMAMC Tribhuvan Univ, Dept Chem, Biratnagar, Nepal

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2024年 / 80卷

关键词：

crystal structure; acylation; thienylallylamines; maleic acid amide; weak interactions; Hirshfeld surface analysis; DERIVATIVES;

D O I：

10.1107/S2056989024005826

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C19H18BrFN2O, the pyrrolidine ring adopts an envelope conformation. In the crystal, molecules are linked by intermolecular N-H center dot center dot center dot O, C-H center dot center dot center dot O, C-H center dot center dot center dot F and C-H center dot center dot center dot Br hydrogen bonds, forming a three-dimensional network. In addition, C-H center dot center dot center dot pi interactions connect molecules into ribbons along the b-axis direction, consolidating the molecular packing. The intermolecular interactions in the crystal structure were quantified and analysed using Hirshfeld surface analysis.

引用

页码：777 / +

页数：11

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