Low cost rotating disc electrode built using accessible hand tools and 3D printing

被引:1
作者
Shnier, Adam [1 ]
Velempini, Tarisai [1 ]
Falch, Anzel [1 ]
机构
[1] Univ Witwatersrand, Mol Sci Inst, Sch Chem, ZA-2050 Johannesburg, South Africa
基金
新加坡国家研究基金会;
关键词
RDE; Electrochemistry; Electrolysis; Education; Rotor; Electrode;
D O I
10.1016/j.ohx.2025.e00626
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
Rotating disc electrodes (RDEs) are ubiquitous among electrochemistry labs for their versatility. They serve to mitigate the mass transport limitations in experiments through hydrodynamic control. Commercially available RDEs cost thousands of USD ($) making them unaffordable for many lower budget research groups or education institutions. Affordable designs exist in literature to make these, but precision machined parts are required. The presented prototype is fabricated using a 3D printed design and common hand tools, providing clean and reproducible data. This facilitates production in a wider range of environments for research and education applications, as is ideal in the South African context in which it was designed.
引用
收藏
页数:23
相关论文
共 36 条
[1]   "The Fe Effect": A review unveiling the critical roles of Fe in enhancing OER activity of Ni and Co based catalysts [J].
Anantharaj, Sengeni ;
Kundu, Subrata ;
Noda, Suguru .
NANO ENERGY, 2021, 80
[2]  
ANGELL DH, 1972, J ELECTROANAL CHEM, V35, P55, DOI 10.1016/S0022-0728(72)80294-8
[3]  
[Anonymous], 2023, NIST
[4]   Hydrodynamic electrochemistry: Design for a high-speed rotating disk electrode [J].
Banks, CE ;
Simm, AO ;
Bowler, R ;
Dawes, K ;
Compton, RG .
ANALYTICAL CHEMISTRY, 2005, 77 (06) :1928-1930
[5]  
BARD AJ, 2001, ELECTROCHEMICAL METH
[6]  
Baur JE, 2007, HANDBOOK OF ELECTROCHEMISTRY, P829, DOI 10.1016/B978-044451958-0.50036-7
[7]  
Beauregard B., 2017, Arduino-PID-library
[8]  
Bio-Logic Science Instruments, 2016, Tech. Rep
[9]   PassStat, a simple but fast, precise and versatile open source potentiostat [J].
Caux, Melicia ;
Achit, Anis ;
Var, Kethsovann ;
Boitel-Aullen, Gabriel ;
Rose, Daniel ;
Aubouy, Agnes ;
Argentieri, Sylvain ;
Campagnolo, Raymond ;
Maisonhaute, Emmanuel .
HARDWAREX, 2022, 11
[10]   PIGMENTS, DYES AND FLUORESCENT BRIGHTENING AGENTS FOR PLASTICS - AN OVERVIEW [J].
CHRISTIE, RM .
POLYMER INTERNATIONAL, 1994, 34 (04) :351-361