Effect of additive content on the microstructure and room-temperature and high-temperature mechanical properties of Si3N4 ceramics

被引:1
作者
Du, Songmo [1 ]
Li, Fei [1 ]
Zhang, Jie [2 ]
Chen, Zhanglin [1 ]
Zhang, Shijia [1 ]
Zhao, Shuo [1 ]
Zhao, Dengke [1 ]
Fan, Binbin [1 ]
Chen, Kexin [3 ]
Liu, Guanghua [1 ]
机构
[1] Tsinghua Univ, Sch Mat Sci & Engn, State Key Lab New Ceram & Fine Proc, Beijing 100084, Peoples R China
[2] Yongjiang Lab, Adv Ceram & Struct Ctr, Ningbo, Peoples R China
[3] Univ Sci & Technol Beijing, State Key Lab Adv Met & Mat, Beijing 100083, Peoples R China
基金
中国国家自然科学基金; 中国博士后科学基金;
关键词
grain growth; mechanical property; silicon nitride; sintering additive content; two-step sintering; SILICON-NITRIDE CERAMICS; ABNORMAL GRAIN-GROWTH; PHASE-TRANSFORMATION; STRENGTH; EVOLUTION;
D O I
10.1111/ijac.15013
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Si3N4 ceramics with uniform grain size distribution were fabricated using spark plasma sintering method and post-heat treatment. The effect of sintering additive content on the grain growth and room-temperature and high-temperature mechanical properties of Si3N4 ceramics were studied. By modulating the competitive growth of beta-Si3N4 grains along the basal and the prism planes, the grains in Si3N4 ceramics were homogeneous. The room-temperature and high-temperature flexural strength of the samples after post-heat treatment were tested. At temperature above 1300 degrees C, the samples with lower sintering additive content exhibit higher strength.
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页数:9
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