SIMULTANEOUS MICROFLUIDIC SYNTHESIS AND SILANIZATION OF IRON OXIDE NANOPARTICLES

被引：0

作者：

Niculescu, Adelina-Gabriela ^{[1
,2
]}

Birca, Alexandra Catalina ^{[1
]}

Morosan, Alina ^{[3
]}

Oprea, Ovidiu Cristian ^{[4
]}

Vasile, Bogdan Stefan ^{[5
,6
]}

Purcareanu, Bogdan ^{[1
,7
]}

Mihaiescu, Dan Eduard ^{[3
]}

Grumezescu, Alexandru Mihai ^{[1
]}

机构：

[1] Natl Univ Sci & Technol Politehn Bucharest, Dept Sci & Engn Oxide Mat & Nanomat, Bucharest, Romania

[2] Univ Bucharest, Res Inst, ICUB, Bucharest, Romania

[3] Natl Univ Sci & Technol POLITEHN Bucharest, Dept Organ Chem, Bucharest, Romania

[4] Natl Univ Sci & Technol POLITEHN Bucharest, Dept Inorgan Chem, Bucharest, Romania

[5] Natl Univ Sci & Technol POLITEHN Bucharest, Natl Res Ctr Micro & Nanomat, Bucharest, Romania

[6] Natl Univ Sci & Technol POLITEHN Bucharest, Res Ctr Adv Mat Prod & Proc, Bucharest, Romania

[7] Biotehnos SA, Otopeni, Romania

来源：

UNIVERSITY POLITEHNICA OF BUCHAREST SCIENTIFIC BULLETIN SERIES B-CHEMISTRY AND MATERIALS SCIENCE | 2025年 / 87卷 / 01期

关键词：

microfluidic synthesis; on-chip functionalization; 3D microfluidic platform; iron oxide nanoparticles; organosilane shell;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Iron oxide nanoparticles (Fe3O4 NPs) have garnered significant attention in recent years due to their favorable physicochemical and biological characteristics, which make them highly versatile for various applications. As a result, there is an increasing focus on optimizing synthesis approaches to ensure they are both more efficient and reproducible. Thus, this study proposes utilizing emerging microfluidic technologies to fabricate uniform core (Fe3O4)-shell (3-aminopropyltriethoxysilane- APTES) NPs with tunable characteristics, accomplishing the material's simultaneous on-chip synthesis and silanization within a 3D microfluidic platform. The synthesized nanomaterials were analyzed using several techniques, including XRD, FT-IR, DLS, TEM, and TG-DSC techniques.

引用

页码：21 / 34

页数：14

共 31 条

[11] Homogeneous NiMoO4-Co(OH)2 bifunctional heterostructures for electrocatalytic oxygen evolution and urea oxidation reaction
Lu, Xinhua
Wang, Tingjian
Cao, Ming
Cheng, Wenjing
Yang, Huimin
Xu, Hui
He, Changchun
Tian, Lin
Li, Zhao
[J]. INTERNATIONAL JOURNAL OF HYDROGEN ENERGY, 2023, 48 (89) : 34740 - 34749
[12] Ultrafast fabrication of nanospherical CoFe alloys for boosting electrocatalytic water oxidation
Lu, Xinhua
Du, Minglin
Wang, Tingjian
Cheng, Wenjing
Li, Jing
He, Changchun
Li, Zhao
Tian, Lin
[J]. INTERNATIONAL JOURNAL OF HYDROGEN ENERGY, 2023, 48 (87) : 34009 - 34017
[13] Moaca E.A., 2018, Iron Ores Iron Oxide Mater, P229, DOI DOI 10.5772/INTECHOPEN.74176
[14] Mohammadi Mohammad, 2024, Int J Pharm, P124142, DOI 10.1016/j.ijpharm.2024.124142
[15] Microwave-Assisted Silanization of Magnetite Nanoparticles Pre-Synthesized by a 3D Microfluidic Platform
Niculescu, Adelina-Gabriela
Morosan, Alina
Birca, Alexandra Catalina
Gherasim, Oana
Oprea, Ovidiu Cristian
Vasile, Bogdan Stefan
Purcareanu, Bogdan
Mihaiescu, Dan Eduard
Radulescu, Marius
Grumezescu, Alexandru Mihai
[J]. NANOMATERIALS, 2023, 13 (20)
[16] A Review of Microfluidic Experimental Designs for Nanoparticle Synthesis
Niculescu, Adelina-Gabriela
Mihaiescu, Dan Eduard
Grumezescu, Alexandru Mihai
[J]. INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES, 2022, 23 (15)
[17] Magnetite nanoparticles: Synthesis methods-A comparative review
Niculescu, Adelina-Gabriela
Chircov, Cristina
Grumezescu, Alexandru Mihai
[J]. METHODS, 2022, 199 : 16 - 27
[18] Fabrication and Applications of Microfluidic Devices: A Review
Niculescu, Adelina-Gabriela
Chircov, Cristina
Birca, Alexandra Catalina
Grumezescu, Alexandru Mihai
[J]. INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES, 2021, 22 (04) : 1 - 26
[19] Increasing Bioavailability of Trans-Ferulic Acid by Encapsulation in Functionalized Mesoporous Silica
Petrisor, Gabriela
Motelica, Ludmila
Ficai, Denisa
Ilie, Cornelia-Ioana
Trusca, Roxana Doina
Surdu, Vasile-Adrian
Oprea, Ovidiu-Cristian
Mirt, Andreea-Luiza
Vasilievici, Gabriel
Semenescu, Augustin
Ficai, Anton
Ditu, Lia-Mara
[J]. PHARMACEUTICS, 2023, 15 (02)
[20] Exploring Structural, Morphological, and Magnetic Properties of Zinc Nickel Ferrites Systems Nanocomposites
Prabakar, Arthur Charles
Killivalavan, Govindarasu
Sivakumar, Dhananjayan
Naidu, K. Chandra Babu
Sathyaseelan, Balaraman
Senthilnathan, Krishnamoorthy
Baskaran, Iruson
Manikandan, Elayaperumal
Balaraju, M.
[J]. BIOINTERFACE RESEARCH IN APPLIED CHEMISTRY, 2021, 11 (01): : 7785 - 7793

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