Effect of Thermal Treatment on the Structure, Microstructure and Magnetic Properties of Co-precipitated CoFe2O4 Nanoparticles

被引:0
作者
Al-Rashidi, Zainab [1 ]
Khmissi, Hammadi [1 ]
El-Ghoul, Jaber [2 ]
Ben Tahar, Lotfi [3 ]
机构
[1] Northern Border Univ, Coll Sci, Dept Phys, Ar Ar, Saudi Arabia
[2] Imam Mohammad Ibn Saud Islamic Univ IMSIU, Coll Sci, Dept Phys, Riyadh 11623, Saudi Arabia
[3] Northern Border Univ, Coll Sci, Dept Chem, Ar Ar, Saudi Arabia
关键词
cobalt ferrite; nanoparticles; thermal treatment; cation's distribution; magnetic properties; FERRITE NANOPARTICLES; PARTICLE-SIZE; TEMPERATURE; WATER; SPECTRA; SPINELS; DESIGN;
D O I
10.1134/S1063782624601493
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
The exceptional chemical and structural stability and the fascinating magnetization effects of Cobalt ferrite, make it a promising candidate for various applications. In this paper, Cobalt ferrite (CoFe2O4) nanoparticles were synthesized by the chemical co-precipitation method and subsequently heat-treated at various temperatures. The elemental chemical composition, structure, morphology, and magnetic properties of the as-prepared cobalt ferrite nanoparticles and those obtained by heat-treating the former at different temperatures were characterized by energy dispersive X-ray analysis (EDX), X-ray diffraction (XRD), Fourier transforms infrared analysis (FTIR), transmission electron microscopy (TEM) and vibrating sample magnetometry (VSM). All samples had a cubic spinal-type structure. The average particles size increased with heat treatment temperature; It ranged from similar to 15 to similar to 35 nm in the temperature range 400-800 degrees C. Magnetic measurements revealed that both saturation magnetization (M-s) and coercivity field (H-c) are reasonably high and were found to increase with increasing temperature. The magnetic behavior of our ferrites was correlated with the XRD and the TEM results.
引用
收藏
页码:620 / 630
页数:11
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