Cleavage of Submicron Solid Films As a Method to Prepare Cross Sections from Heterostructures for High-Resolution Transmission Microscopy

被引:0
作者
Vorob'ev, A. B. [1 ]
Gutakovsky, A. K. [1 ]
Prinz, V. Ya. [1 ]
机构
[1] Russian Acad Sci, Rzhanov Inst Semicond Phys, Siberian Branch, Novosibirsk 630090, Russia
关键词
transmission electron microscopy; atomic resolution; free-standing thin film; cross section; brittle crack; cleavage; EPITAXIAL GAAS/ALAS SUPERLATTICES; INTERFACE STRUCTURE; QUANTUM-WIRE; RECONSTRUCTION; SEMICONDUCTORS; GAAS(311); QUALITY;
D O I
10.3103/S8756699024700511
中图分类号
O4 [物理学];
学科分类号
0702 ;
摘要
A method of preparation, which makes it possible to form defectless cross sections for transmission electron microscopy from heterostructures and ensures atomic resolution over a larger surface area, is described in details. The method is illustrated with examples of studies on complexly shaped heterointerfaces and selective oxidation and selective etching of superlattices.
引用
收藏
页码:447 / 456
页数:10
相关论文
共 24 条
[1]   OPTICAL-PROPERTIES OF A HIGH-QUALITY (311)-ORIENTED GAAS/AL0.33GA0.67AS SINGLE-QUANTUM-WELL [J].
BRANDT, O ;
KANAMOTO, K ;
TOKUDA, Y ;
TSUKADA, N ;
WADA, O ;
TANIMURA, J .
PHYSICAL REVIEW B, 1993, 48 (23) :17599-17602
[2]   Analysis of GaAs substrate removal etching with citric acid:H2O2 and NH4OH:H2O2 for application to compliant substrates [J].
CarterComan, C ;
BicknellTassius, R ;
Benz, RG ;
Brown, AS ;
Jokerst, NM .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 1997, 144 (02) :L29-L31
[3]   Step structure on GaAs(113)A studied by scanning tunneling microscopy [J].
Geelhaar, L ;
Márquez, J ;
Jacobi, K .
PHYSICAL REVIEW B, 1999, 60 (23) :15890-15895
[4]   MOLECULAR-BEAM EPITAXIAL GAAS/ALAS SUPERLATTICES IN THE (311)-ORIENTATION [J].
HSU, Y ;
WANG, WI ;
KUAN, TS .
PHYSICAL REVIEW B, 1994, 50 (07) :4973-4975
[5]   Study of interface abruptness of molecular beam epitaxial GaAs/AlAs superlattices grown on GaAs(311) and (100) substrates [J].
Hsu, Y ;
Wang, WI ;
Kuan, TS .
JOURNAL OF VACUUM SCIENCE & TECHNOLOGY B, 1996, 14 (03) :2286-2289
[6]   Sample preparation of InGaAsP/InP-based lasers for plan-view transmission electron microscopy using selective chemical thinning [J].
Kallstenius, T .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 1999, 146 (02) :758-760
[7]   A new specimen preparation method for cross-section TEM using diamond powders [J].
Kawasaki, M ;
Yoshioka, T ;
Shiojiri, M .
JOURNAL OF ELECTRON MICROSCOPY, 1999, 48 (02) :131-137
[8]   Interface structure and growth mode of quantum wire and quantum dot GaAs-AlAs structures on corrugated (311)A surfaces [J].
Ledentsov, NN ;
Litvinov, D ;
Rosenauer, A ;
Gerthsen, D ;
Soshnikov, IP ;
Shchukin, VA ;
Ustinov, VM ;
Egorov, AY ;
Zukov, AE ;
Volodin, VA ;
Efremov, MD ;
Preobrazhenskii, VV ;
Semyagin, BP ;
Bimberg, D ;
Alferov, ZI .
JOURNAL OF ELECTRONIC MATERIALS, 2001, 30 (05) :463-470
[9]   SMALL-ANGLE CLEAVAGE OF SEMICONDUCTORS FOR TRANSMISSION ELECTRON-MICROSCOPY [J].
MCCAFFREY, JP .
ULTRAMICROSCOPY, 1991, 38 (02) :149-157
[10]   Absence of long-range ordered reconstruction on the GaAs(311)A surface [J].
Moriarty, P ;
Ma, YR ;
Dunn, AW ;
Beton, PH ;
Henini, M ;
McGinley, C ;
McLoughlin, E ;
Cafolla, AA ;
Hughes, G ;
Downes, S ;
Teehan, D ;
Murphy, B .
PHYSICAL REVIEW B, 1997, 55 (23) :15397-15400