Determination of antibiotic residues in pork meat from Northeast Mexico by UPLC-MS

被引：0

作者：

Paz-Gonzalez, Alma D. ^{[1
,2
]}

Martinez-Vazquez, Ana V. ^{[3
]}

Ortiz-Perez, Eyra ^{[2
]}

Ramirez-Martinez, Carlos ^{[1
]}

Lara-Ramirez, Edgar E. ^{[2
]}

Juarez-Rendon, Karina ^{[3
]}

Bocanegra-Garcia, Virgilio ^{[3
]}

Vazquez, Karina ^{[1
]}

Rivera, Gildardo ^{[2
]}

机构：

[1] Univ Autonoma Nuevo Leon, Fac Med Vet & Zootecnia, Gral Escobedo, Mexico

[2] Inst Politecn Nacl, Ctr Biotecnol Genomica, Lab Biotecnol Farmaceut, Blvd Maestro,S-N Esq Elias Pina, Reynosa 88710, Mexico

[3] Inst Politecn Nacl, Ctr Biotecnol Genom, Reynosa, Mexico

来源：

CYTA-JOURNAL OF FOOD | 2024年 / 22卷 / 01期

关键词：

Antibiotics; minimum residues limits; pork meat; UPLC-MS; SOLID-PHASE EXTRACTION; LIQUID-CHROMATOGRAPHY; TETRACYCLINE ANTIBIOTICS; SULFONAMIDE RESIDUES; MODIFIED QUECHERS; DRUG RESIDUES; BETA-LACTAM; FOOD; CHICKEN; MUSCLE;

D O I：

10.1080/19476337.2024.2413950

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

In this study, the aim was to identify and quantify antibiotic residues in pork meat samples of supermarkets and butcher shops of two main cities in northeast Mexico, using Ultra-Performance Liquid Chromatography-Mass Spectrometry (UPLC-MS). The results shown seven antibiotic residues detected in the samples. Ampicillin was the main antibiotic with a higher positive rate (>59%) in supermarkets and butcher shops. Tetracycline and sulfamethazine had a high positive rate (>25%). Finally, the quantification of antibiotics shown a high positive rate of samples that exceed the minimum residues limits (MRL). The high positive rate of antibiotic residues in this study suggests an inadequate management in the food industry and represents a potential risk for the human health in the northeast from Mexico.

引用

页数：10

共 53 条

[1] [Anonymous], 2010, Carte dAlea Seismique (Rapport technique), P1
[2] The public health issue of antibiotic residues in food and feed: Causes, consequences, and potential solutions
Arsene, Mbarga Manga Joseph
Davares, Anyutoulou Kitio Linda
Viktorovna, Podoprigora Irina
Andreevna, Smolyakova Larissa
Sarra, Souadkia
Khelifi, Ibrahim
Sergueievna, Das Milana
[J]. VETERINARY WORLD, 2022, 15 (03) : 662 - 671
[3] Bermúdez-Almada MD, 2001, REV CIENT-FAC CIEN V, V11, P127
[4] Bn C., 2023, Resilience and food security in a food systems context (p. 413), DOI [https://doi.org/10.1007/978-3-031-23535-1, DOI 10.1007/978-3-031-23535-1]
[5] Carrillo H. H. G., 2004, Veterinaria Mxico, V35, P91
[6] Pesticides, environment, and food safety
Carvalho, Fernando P.
[J]. FOOD AND ENERGY SECURITY, 2017, 6 (02): : 48 - 60
[7] Determination of veterinary antibiotics in cow milk using rotating-disk sorptive extraction and liquid chromatography
Castillo-Aguirre, Alver
Canas, Alejandro
Honda, Luis
Richter, Pablo
[J]. MICROCHEMICAL JOURNAL, 2021, 162
[8] Screening of multi-class antibiotics in pork meat by LC-Orbitrap-MS with modified QuEChERS extraction
Chen, Qing
Pan, Xiao-Dong
Huang, Bai-Fen
Han, Jian-Long
Zhou, Biao
[J]. RSC ADVANCES, 2019, 9 (48) : 28119 - 28125
[9] Rapid determination of sulfonamide residues in pork by surface-modified hydrophilic electrospun nanofibrous membrane solid-phase extraction combined with ultra-performance liquid chromatography
Chen, Rong
Yang, Yingying
Qu, Bin
Li, Yue
Lu, Yong
Tian, Lingling
Shen, Weiyang
Ramakrishna, Seeram
[J]. ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2016, 408 (20) : 5499 - 5511
[10] Codex Alimentarius International Food Standars Maxium Residue Limits (MRLs) and Risk Management Recommendation (RMRs) For Residues of Veterinary Drugs in Food, 2021, CX/MRL 2-2021 (pp. 149)

← 1 2 3 4 5 6 →