HS-SPME-GC-MS Analysis of Volatile Compounds in Whole-Fat Cow and Goat Milk Powder during Accelerated Oxidation

被引:0
作者
Xue H. [1 ]
Li X. [1 ]
Meng Y. [2 ]
He B. [3 ]
Zhang L. [1 ]
Liu X. [1 ]
Ma J. [1 ]
机构
[1] School of Food Science and Engineering, Shaanxi University of Science and Technology, Xi’an
[2] Shaanxi Jinniu Dairy Co. Ltd., Weinan
[3] College of Bioresources Chemical and Materials Engineering, Shaanxi University of Science and Technology, Xi’an
来源
Shipin Kexue/Food Science | 2024年 / 45卷 / 10期
关键词
headspace solid-phase microextraction coupled with gas chromatography-mass spectrometry; volatile compounds; whole-fat cow milk powder; whole-fat goat milk powder;
D O I
10.7506/spkx1002-6630-20230929-262
中图分类号
学科分类号
摘要
In order to investigate the changes of flavor substances in whole-fat cow and goat milk powder during storage, the volatile compounds of whole-fat cow and goat milk powder during accelerated oxidation were analyzed using headspace solid-phase microextraction coupled with gas chromatography-mass spectrometry (HS-SPEM-GC-MS). The results indicated that 56 and 63 volatile substances were identified in whole-fat cow and goat milk powder, respectively, mainly including acids, alcohols, carbonyls, esters, aromatics and heterocyclic compounds. Ten significantly differential volatile compounds were identified between whole-fat cow and goat milk powder by principal component analysis (PCA) and cluster analysis (CA). The relative content of butyric acid decreased and the relative content of 2-nonanone and 1-chloropentane increased in whole-fat cow milk powder during accelerated storage. The relative contents of nonanaldehyde, octanoic acid, propionic acid, and butylhydroxytoluene decreased, and the relative contents of benzaldehyde, 2-heptanone, and allyl n-propyl ester increased in whole-fat goat milk powder. © 2024 Chinese Chamber of Commerce. All rights reserved.
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页码:272 / 280
页数:8
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