Effect of doped chromium oxide and graphene on microstructure and properties of tritium-blocking coatings on micro-arc alumina

被引:0
作者
Yang, Han [1 ]
Feng, Jun [1 ]
Jian, Fenglin [1 ]
Yang, Xudong [1 ]
Wang, Jun [1 ]
机构
[1] School of Mechanical Engineering, University of South China, Hunan, Hengyang
关键词
1060 pure aluminum; Cr[!sub]2[!/sub]O[!sub]3[!/sub; graphene; micro-arc oxidation; tritium-blocking coating;
D O I
10.11868/j.issn.1001-4381.2023.000618
中图分类号
学科分类号
摘要
In order to obtain high quality aluminium oxide tritium barrier coatings, micro-arc oxidation (MAO)technology was used to prepare micro-arc oxidation coatings on the surface of 1060 pure aluminium by doping Cr2O3 and graphene as additives in the electrolyte, using phosphate as the main electrolyte component. The surface morphology, elemental distribution, physical phase composition, thickness,hardness, abrasion and corrosion resistance of the micro-arc oxidation coatings were characterized by scanning electron microscope,X-ray diffractometer,eddy current thickness gauge,Vickers hardness tester, friction and wear tester, and electrochemical workstation. The results show that the surface morphology of the micro-arc oxidation coatings prepared by adding 3 g/L Cr2O3 and 1 g/L graphene into the electrolyte is more dense, and the proportion of α-Al2O3 and γ-Al2O3 in the coatings increases, with the thickness reaching 25.3 μm,the hardness reaching 763.01HV, and the average friction coefficient of 0.4781.At the same time,the self-corrosion potential is -0.185 V, and the self-corrosion current density is 1.095×10-9 A·cm-2 © 2024 Science Press. All rights reserved.
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页码:151 / 158
页数:7
相关论文
共 25 条
  • [1] NIE B J, RAN G M, Qet al ZENG, Insights into fuel start-up and self-sufficiency for fusion energy:the case of CFETR, Energy Science and Engineering, 7, pp. 457-468, (2019)
  • [2] WU Y, CHEN Z, HU Let, Identification of safety gaps for fusion demonstration reactors, Nature Energy, 1, pp. 1-11, (2016)
  • [3] WANG L, WU Y Y, LUO X Fet al., Effects of Ar/O2 ratio on preparation and properties of multilayer Cr2O3/α-Al2O3 tritium permeation barrier, Surface & Coatings Technology, 339, pp. 132-138, (2018)
  • [4] Ti/AlN/Ti/AlN多层涂层的制备和阻氘性能, 稀有金属材料与工程, 51, pp. 3943-3948, (2022)
  • [5] 43, pp. 872-884, (2019)
  • [6] WALLIN E, ANDERSSON J M, LATTERMANN Met al, Influence of residual water on magnetron sputter deposited crystalline Al2O3 thin films, Thin Solid Films, 516, pp. 3877-3883, (2008)
  • [7] HE D, LEI Y, ZHANG Cet al, Deuterium permeation of Al2O3/Cr2O3 composite film on 316L stainless steel, International Journal of Hydrogen Energy, 40, pp. 2899-2903, (2015)
  • [8] SU Y, KRAVETS V G, WONG S, Impermeable barrier films and protective coatings based on reduced graphene oxide, Nature Communications, 5, pp. 1-5, (2014)
  • [9] (2020)
  • [10] 47, pp. 50-62, (2019)