A high-yielding synthetic method for the condensates of threo-(1S,2S)-2-amino-1-4'-nitrophenyl-1,3-propanediol and some ketones

被引：0
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作者：
Shan, Z.-X. [1 ]
Wan, B.-Y. [1 ]
Wang, G.-P. [1 ]
机构：
[1] Coll. of Chemistry and Molecule Sci., Wuhan University, Wuhan 430072, Hubei, China
来源：
Wuhan Daxue Xuebao/Journal of Wuhan University | 2001年 / 47卷 / 02期
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摘要：
A convenient preparative method of the condensates of threo- (1S,2S)-2-amino-1-4'-nitrophenyl-1,3-propanediol with some ketones was described. Threo-(1S,2S)-2-amino-1-4'-nitrophenyl-1, 3-propanediol reacted azeotropically with some aliphatic ketones or alicyclic ketones in toluene or xylene, and then treated with diethyl ether to offer almost quantitatively crystalline condensates.
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页码：165 / 168
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