Fabrication and characterization of (Bi,Pb)-Sr-Ca-Cu-O (2223) bars

被引:0
作者
Chudzik, M.P. [1 ]
Polzin, B.J. [1 ]
Thayer, R. [1 ]
Picciolo, J.J. [1 ]
Fisher, B.L. [1 ]
Lanagan, M.T. [1 ]
机构
[1] Argonne Natl Lab, Argonne, United States
来源
IEEE Transactions on Applied Superconductivity | 1997年 / 7卷 / 2 pt 2期
关键词
Bars (metal) - Critical current density (superconductivity) - Differential thermal analysis - Hot pressing - Microstructure - Phase composition - Scanning electron microscopy - Sintering - Thermal conductivity of solids - X ray diffraction analysis;
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摘要
Bulk bars for current lead applications were fabricated from (Bi,Pb)-Sr-Ca-Cu-O (Bi-2223) for low thermal conductivity and high critical current. Bars measuring 17.8 cm in length were made by uniaxially pressing Bi-2223 powder of controlled (1.7/0.34)223 and (1.8/0.4)223 phase composition. The bulk bars were densified by subjecting them to a schedule of alternate liquid-phase sintering and cold isostatic pressing. Liquid-phase sintering temperatures were optimized from differential thermal analysis and microstructure morphology. Phase purity and microstructure were evaluated by X-ray diffraction and scanning electron microscopy. Low-resistance silver contacts were applied to the bars by hot-pressing at 820 °C and 3 MPa. Critical current densities 1000 A/cm2 (critical currents of 750 A at 77 K in self-field conditions) were achieved.
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页码:2102 / 2105
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