Synthesis of 1-(Adamantyl-1)-2n-Hexafluoropropane.

被引：0

作者：

Morozov, V.A.

Fedotov, A.K.

Zamyslov, R.A.

Dobrov, I.V.

Podkhalyu Zin, A.T.

机构：

来源：

Khimicheskaya Promyshlennost' | 1980年 / 03期

关键词：

CHEMICAL REACTIONS - Synthesis - RADIATION EFFECTS;

D O I：

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学科分类号：

摘要：

A study was made of the synthesis of 1(adamantyl-1)-2n-hexafluoropropane by gamma -initiated alkylation of adamantane by hexafluoropropylene. A technological scheme for the synthesis of fluoroalkyladamantanes by radiation-chemical alkylation has been developed. An experimental batch of product has been obtained using cyclohexane as the solvent. An optimization of the process is carried out for a reactor with an output of 30 tons/year.

引用

页码：146 / 147