Synthesis, characterization and thermal decomposition of M1[M2(C2O4)2]&middotxH2O (x=5 for M1=Co and x=4 for M1=Cd; M2=Ni)

被引：0
|
作者：
Deb, N. [1 ]
Baruah, S.D. [2 ]
Dass, N.N. [3 ]
机构：
[1] Department of Chemistry, N. E. Regl. Inst. Sci. and Technol., Nirjuli 791109 Arunachal Pradesh, India
[2] Regional Research Laboratory, Jorhat 785006, Assam, India
[3] Department of Chemistry, Dibrugarh University, Dibrugarh 786004, Assam, India
来源：
Journal of Thermal Analysis and Calorimetry | 2000年 / 59卷 / 03期
关键词：
Air - Cadmium compounds - Cobalt compounds - Differential scanning calorimetry - Infrared spectroscopy - Light reflection - Magnetic properties - Mixtures - Nitrogen - Pyrolysis - Structure (composition) - Synthesis (chemical);
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学科分类号：
摘要：
Cobalt bis(oxalato)nickelate pentahydrate, Co[Ni(C2O4)2]&middot5H2O and cadmium bis(oxalato)nickelate tetrahydrate, Cd[Ni(C2O4)2]&middot4H2O have been synthesized and characterized by elemental analysis, reflectance and IR spectral studies. Thermal decomposition studies (TG, DTG and DTA) in air showed that both the compound of cobalt and cadmium produced the oxide, MNiOx (x=3 for M=Co; x=2 for M=Cd) at 325 and 360°C respectively. DSC studies in nitrogen attributed only the mixture of both the metal at the end.
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页码：791 / 797
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