From Butadiynyl (-CtC-CtCR) Ligands to Alkylidyne-Carbides: Synthesis and Characterisation of the Unusual Hexanuclear Ruthenium Carbido Clusters [Ru6(CO)13(ae-CO)2(ae-PPh2)(ae5- C)(ae3$ MIN@C-CtCR)] (R = But, Ph)

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Blenkiron, P.

Taylor, N. J.

Carty, A. J.

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Journal of Polymer Materials | 1994年 / 11卷 / 02期

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[1] FROM BUTADIYNYL (-C-C-C-CR) LIGANDS TO ALKYLIDYNE-CARBIDES - SYNTHESIS AND CHARACTERIZATION OF THE UNUSUAL HEXANUCLEAR RUTHENIUM CARBIDO CLUSTERS [RU-6(CO)(13)(MU-CO)(2)(MU-PPH(2))(MU-5-C)(MU(3)-C-C-CR)] (R=BU(T), PH)
BLENKIRON, P
TAYLOR, NJ
CARTY, AJ
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[2] High-pressure synthesis of [Ru2(ae-dppm): (ae-CO)(CO)4, Ru2(ae-dppm)(ae-dmpm) (ae-CO)(CO)4], and [Ru(dcypm)(CO)3] from Ru3(CO)12 and the diphosphines: R2PCH2PR2; R = CH3(dmpm), C6H5 (dppm) and C6H11 (dcypm). Crystal and molecular structures of [Ru2(ae-dppm)2(ae-CO)(CO)4], and [Ru (dcypm)(CO)3]
Polyhedron, 9 (1453):
[3] Reactions of Ru3(ae-dppm)(CO)10 with unsaturated hydrocarbons Cycloocta-1,3,5,7-tetraene X-ray structures of Ru3(ae-dppm)(ae-C8H8)(CO)6, Ru3(ae3-PPhCH2PPh2)(ae3-C8H8 )(Ph)(CO)5 , Ru3{ae3-PPhCH2 PPh(C6H4)}(ae-C8H8)(ae-CO)(CO)4 , and Ru3(ae-H){ae3-PPh2CHPPh(C6H4)$R TBC@(ae-C 8H9)(ae-CO)(CO)4
Journal of Organometallic Chemistry, 526 (01):
[4] Construction of unusual cluster geometries about a dicarbon ligand: reactions of Ru5(ae5-C2)(ae-SMe)2(ae-PPh2)2(CO)11 with iron or ruthenium carbonyls
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[5] New ruthenium-tin clusters with bulky ligands. Crystal and molecular structures of [Ru2(CO)6(ae-SnR2)- (ae-Ph2PCH2PPh2)], [Ru3(CO),- (ae-SnR'2)3], [Ru3(CO)9(ae-SnR'2)3], [Ru3(CO)9(ae-SnR'2)-(ae-SnR'2)2] and [Ru3(CO)9(ae-SnR'2)22-(ae-SnR'2 )] [R = CH(SiMe3)2, R' = C6H2Pri3-2,4,6]
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[6] Synthesis, structural characterisation and nuclear magnetic resonance study of (Ru6C(CO)15(ae3-eta1:eta2:eta2-C$ -16$/H16 -ae-O)]: an intermediate in the formation of [Ru6,C(CO)14(ae3-eta2:eta2:eta2$MI N@C16H 16)]
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[7] Oxo ligands as assembling units in mixed-metal cluster chemistry: synthesis and X-ray structure of the bow-tie cluster [Mo2Ru3(ae3-O)2(ae3-CPh)(ae-C 3Ph3)( CO)8(eta-C5H5)2]
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[8] Reactions of [eta5-RC5H4 (CO)2Mo]2 (MotMo) With (ae-PhSe)2Fe2 (CO)6. Synthesis and Characterization of Selenolato-Bridged Transition Metal Complexes [eta5-RC5H4Mo (CO) (ae-SePh)]2 (R = MeCO, MeO2C) and eta5-RC5H4MoFe2 (CO)4 (ae3-Se) [ae, eta1: eta2-C(O)Ph](ae-SePh)2 (R = MeCO, EtO2C)
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Wang, J.-Q.
Hu, Q.-M.
Sun, J.
Journal of Coordination Chemistry., 1997, 42 (1-2)
[9] Synthesis, structure and reactivity of triosmium clusters derived from the reactions of [Os3(CO)10(ae-@dppm)] (dppm = Ph2PCH2PPh2) and [Os3-@(ae-@H)(CO)8{Ph2PCH2P(Ph)C6H4 $ RTBC@] with PHPh2
J Chem Soc Dalton Trans, 7 (1097):
[10] AN UNUSUAL ELECTRON-RICH CARBIDO PLATINUM RUTHENIUM CLUSTER FROM THE REACTION OF DIPHENYLACETYLENE WITH PTRU5(CO)16(MU-6-C) - SYNTHESIS AND CRYSTALLOGRAPHIC CHARACTERIZATIONS OF PTRU5(CO)13(MU-PHC2PH)(MU-3-PHC2PH)(MU-5-C) AND RU6(CO)13(MU-3-PHC2PH)2(MU-6-C)
ADAMS, RD
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ORGANOMETALLICS, 1993, 12 (04) : 1238 - 1242