This report describes an investigation carried out into methods of disposing of cyanide containing wastes from the metal finishing industry - in particular heat treatment salt residues. The object of the investigation was to select the method most economically and environmentally acceptable, and most suited for operation at a treatment center. A process of electrolytic oxidation appeared the most promising of the methods under consideration and a series of laboratory and pilot plant studies were undertaken which culminated in the construction and commercial operation of a 5,000 amp unit capable of treating 330 tons heat treatment residues per year.