Effect of temperature on the purity of product in the preparation of 1-butyl-3-methylimidazolium-based ionic liquids

被引：0
|
作者：
Kärkkäinen, Johanna [1 ]
Asikkala, Janne [1 ]
Laitinen, Risto S. [1 ]
Lajunen, Marja K. [1 ]
机构：
[1] Department of Chemistry, University of Oulu, P. O. Box 3000, 90014 Oulu, Finland
来源：
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences | 2004年 / 59卷 / 07期
基金：
芬兰科学院;
关键词：
Mass spectrometry - Chlorine compounds - Electrospray ionization;
D O I：
10.1515/znb-2004-0704
中图分类号：
学科分类号：
摘要：
The preparation of room-temperature ionic liquids 1-butyl-3- methylimidazolium chloride, hexafluorophosphate, and dicyanamide by microwave-assisted reaction in non-solvent and solvent conditions has been studied in this contribution. A special emphasis is put on the effect of the reaction temperature on the purity of ionic liquids that was monitored by electrospray ionisation mass spectrometry and 1H NMR. The X-ray structure of 1-butyl-3-methylimidazolium chloride is presented.
引用
收藏
页码：763 / 770
相关论文
共 50 条
  • [1] Effect of temperature on the purity of product in the preparation of 1-butyl-3-methylimidazolium-based ionic liquids
    Kärkkäinen, J
    Asikkala, J
    Laitinen, RS
    Lajunen, MK
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 2004, 59 (07): : 763 - 770
  • [2] Recovery of 1-butyl-3-methylimidazolium-based Ionic Liquids
    Idaham, Nurul Fasihah
    Bustam, Mohamad Azmi
    Kait, Chong Fai
    Man, Zakaria
    ADVANCED MATERIALS CONFERENCE (AMC 2012), 2014, 879 : 230 - +
  • [3] Study on the Recovery of 1-butyl-3-methylimidazolium-based Ionic Liquids
    Idaham, Nurul Fasihah
    Khalil, Mohamad Azmi Bustam
    Kait, Chong Fai
    PROCESS AND ADVANCED MATERIALS ENGINEERING, 2014, 625 : 144 - +
  • [4] Effect of Counteranions on the Conformational Equilibrium of 1-Butyl-3-methylimidazolium-Based Ionic Liquids
    Hatano, Naohiro
    Takekiyo, Takahiro
    Abe, Hiroshi
    Yoshimura, Yukihiro
    INTERNATIONAL JOURNAL OF SPECTROSCOPY, 2011,
  • [5] Interaction of copper with dinitrogen tetroxide in 1-butyl-3-methylimidazolium-based ionic liquids
    Morozov, I. V.
    Deeva, E. B.
    Glazunova, T. Yu.
    Troyanov, S. I.
    Guseinov, F. I.
    Kustov, L. M.
    DALTON TRANSACTIONS, 2017, 46 (13) : 4430 - 4434
  • [6] New Insights into the Thermal Stability of 1-Butyl-3-methylimidazolium-Based Ionic Liquids
    Belesov, Artyom, V
    Shkaeva, Natalya, V
    Popov, Mark S.
    Skrebets, Tatyana E.
    Faleva, Anna, V
    Ul'yanovskii, Nikolay, V
    Kosyakov, Dmitry S.
    INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES, 2022, 23 (18)
  • [7] Influence of anionic structure on the dissolution of chitosan in 1-butyl-3-methylimidazolium-based ionic liquids
    Chen, Qingtai
    Xu, Airong
    Li, Zhiyong
    Wang, Jianji
    Zhang, Suojiang
    GREEN CHEMISTRY, 2011, 13 (12) : 3446 - 3452
  • [8] VLE measurement of binary systems 1-butyl-3-methylimidazolium-based ionic liquids and ethanol or water
    Graczova, Elena
    Steltenpohl, Pavol
    JOURNAL OF CHEMICAL THERMODYNAMICS, 2024, 188
  • [9] Thermodynamic modeling of CO2 absorption in 1-butyl-3-methylimidazolium-based ionic liquids
    Bazargani, Zohreh
    Sabzi, Fatemeh
    JOURNAL OF MOLECULAR LIQUIDS, 2016, 223 : 235 - 242
  • [10] Use of 1-butyl-3-methylimidazolium-based ionic liquids as methane hydrate inhibitors at high pressure conditions
    Sanches de Menezes, Davi Eber
    Pessoa Filho, Pedro de Alcantara
    Robustillo Fuentes, Maria Dolores
    CHEMICAL ENGINEERING SCIENCE, 2020, 212
12345