Coulometric determination of water in lubricating greases

被引：0

作者：

Kil'yanov, M.Yu. ^{[1
]}

Petrov, S.I. ^{[1
]}

Chaduneli, Z.K. ^{[1
]}

机构：

[1] I.M. Gubkin Inst of Oil & Gas, Russia

来源：

Chemistry and Technology of Fuels and Oils | 1988年 / 23卷 / 9-10期

关键词：

Chemical Analysis - Titration - Coulometers - Performance - Lubricants - Analysis - Water - Analysis;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

The feasibility of using a coulometric titration version of the Fischer method to determine water content in several greases was studied. A modified Fischer reagent was used in which methanol was replaced by ethylcellosolve to eliminate the side reactions generated by methanol, reduce reagent toxicity, and broaden the field of reagent application. A coulometric cell was designed to diminish solution mixing between the anode and cathode sides. The relative standard deviation of the method was 0.005-0.018%.

引用

页码：500 / 501