Controlled hydrolysis reactions of the Group 15 element-azamacrocyclic complexes MCl3L (M = As, Sb or Bi; L = 1,4,7-trimethyl-1,4,7- triazacyclononane). Formation and crystal structures of [AsCl2L][As2OCl], [H2L]2[Sb2OCl6]Cl2, [HL]I and [H2L]2[Sb2Cl]CluMeCN-H2O