We thank Th. Peun and P. Zinn as well as J. Otto and M. Winzenick for their very valuable advice throughout the course of experiments at MAX 80 (HASYLAB;
beamline F2/1) and at beamline F3;
respectively. Useful discussions with M. Cramm are also acknowledged. The work was supported by the Deutsche Forschungsgemeinschaft;
the BMBF (No. 13N6583);
the Ministerium für Wissenschaft und Forschung NRW and the Fonds der Chemischen Industrie;