Effects of process parameters on the microstructure and properties of LaNiO3 thin films

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作者
Key Laboratory for Thin Film and Microfabrication Technology, Research Institute of Micro/Nanometer Science and Technology, Shanghai Jiaotong University, Shanghai 200030, China [1 ]
不详 [2 ]
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来源
Gongneng Cailiao | 2008年 / 1卷 / 48-50期
关键词
Annealing - Characterization - Chemical analysis - Electric conductivity - Lanthanum compounds - Microstructure - Nickel compounds - Oxygen - Partial pressure - Sputter deposition - Stoichiometry;
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摘要
LaNiO3 thin films have been prepared by RF sputtering and then crystallized after post-annealing. The resistivity was characterized by four probe measurements. The influence of process parameters such as oxygen partial pressure, sputtering power and post-annealing on the microstructure and properties were investigated by XRD, ICP-AES, AFM respectively. It is found that the film was crystallized when annealing at 550°C, however, annealing at 700°C produced better electrical properties and smooth surface. When the oxygen partial pressure is kept between 10% to 25%, the content ratio of La to Ni is of the stoichiometric composition. The resistivity increased with increasing oxygen partial pressure.
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