Evolution of grain boundary character distributions in Pb alloy during high temperature annealing

被引:0
|
作者
Xia, Shuang [1 ]
Zhou, Bangxin [1 ]
Chen, Wenjue [1 ]
Wang, Weiguo [2 ]
机构
[1] Institute of Materials, Shanghai University, Shanghai 200072, China
[2] School of Mechanical Engineering, Shandong University of Technology, Zibo 255049, China
来源
Jinshu Xuebao/Acta Metallurgica Sinica | 2006年 / 42卷 / 02期
关键词
Backscattering - Cold rolling - Crystal orientation - Electron diffraction - Grain boundaries - Optical microscopy - Recrystallization (metallurgy) - Thermomechanical treatment;
D O I
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中图分类号
学科分类号
摘要
Grain boundary character distributions (GBCD) in Pb alloy after thermomechanical treatments were analyzed by electron back scatter diffraction (EBSD) and orientation imaging microscopy (OIM). The frequencies of low ∑ coincidence site lattice (CSL) grain boundaries in Pb-alloy can be enhanced to more than 70% after proper cold rolling combined with annealing at high temperature (0.9Tm) for a very short period of time. Together with ∑1 boundaries, the ∑3 boundaries appeared during recovering. The development of ∑3 boundaries in the primary stage of recrystallization is the main reason for enhancing the frequencies of low ∑ CSL grain boundaries. Triple junctions contained three CSL grain boundaries could be easily found in the OIM map of the specimen with high frequencies of low ∑ CSL grain boundaries, and there are specific orientation relationships among the grains assembled by the triple junctions.
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页码:129 / 133
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