Preparation process of hydrophobic micro-porous waxy corn starch

被引:0
作者
Tang, Hongbo [1 ]
Wang, Xiaoyu [1 ]
Li, Yanping [1 ]
Dong, Siqing [1 ]
机构
[1] Science School, Shenyang University of Technology
来源
Nongye Gongcheng Xuebao/Transactions of the Chinese Society of Agricultural Engineering | 2012年 / 28卷 / 15期
关键词
Hexamethyl disilazane; Hydrophobicity; Modification; Optimization; Starch;
D O I
10.3969/j.issn.1002-6819.2012.15.043
中图分类号
学科分类号
摘要
The hydrophobic modification of micro-porous waxy corn starch was carried out to enhance its oil absorption rate and improve its application quality by using the wet method. Some factors affecting the oil absorption rate of hydrophobic micro-porous waxy corn starch were: reaction temperature, reaction time, pH value and amount of hydrophobic agent. The microstructure and thermal property were characterized and measured by infrared spectrogram, thermogravimetric analyzer and differential scanning calorimetry, respectively. The results indicated that the oil absorption rate of hydrophobic micro-porous waxy corn starch increased by 43.0%, compared with that of micro-porous waxy corn starch. The optimum process conditions for preparing hydrophobic micro-porous waxy corn starch were as follows: reaction temperature 50°C, reaction time 4 h, pH value 9.0. The peak onset temperature, peak temperature, peak end temperature, enthalpy change of DSC curve of hydrophobic micro-porous waxy corn starch decreased, and the thermal stability of hydrophobic micro-porous waxy corn starch decreased, compared with those of micro-porous waxy corn starch. The research results can provide a reference for the commercial applications of the micro-porous waxy corn starch.
引用
收藏
页码:270 / 275
页数:5
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  • [1] Qian J., Chen X., Ying X., Et al., Optimization of porous starch preparation by ultrasonic pretreatment followed by enzymatic hydrolysis, International Journal of Food Science and Technology, 46, 1, pp. 179-185, (2011)
  • [2] Liu S., Wang C., Process of preparation and application about microporous starch, Cereals and Oils Processing, 32, 3, pp. 59-62, (2007)
  • [3] Zhang S., Wang Z., Liu C., Et al., Researches on production craft of microporous starch of unpolished rice, Academic Periodical of Farm Products Processing, 5, pp. 51-54, (2007)
  • [4] Peter R.C., Jiugao Y., Xiaofei M., Preparation of porous starch and its use as a structure-directing agent for production of porous zinc oxide, Carbohydrate Polymers, 83, 2, pp. 1016-1019, (2011)
  • [5] Yao W., Yao H., Adsorbent characteristics of porous starch, Starch/Stǎrke, 54, 6, pp. 260-263, (2002)
  • [6] Yuan M., Wu X., Review on porous starch, Journal of Hebei Agricultural Sciences, 14, 3, (2010)
  • [7] Glenn G.M., Klamczynski A.P., Woods D.F., Et al., Encapsulation of plant oils in porous starch microspheres, Journal of Agricultural and Food Chemistry, 58, 7, pp. 4180-4184, (2010)
  • [8] Liu X., Zhou Q., Zhou C., Et al., Preparation of microporous starch with high oil-absorption capability, Journal of the Chinese Cereals and Oils Association, 20, 3, pp. 22-25, (2005)
  • [9] Wu Y., Du X., Ge H., Et al., Preparation of microporous starch by glucoamylase and ultrasound, Starch/Stǎrke, 63, 4, pp. 217-225, (2011)
  • [10] Xiao H., Lin Q., Wu Y., Et al., Physicochemical properties of porous starches from different botanical origin, Advanced Materials Research, 159, pp. 363-370, (2011)