Fabrication of yttrium aluminum garnet nanofibers by an electrospinning technique

被引：0

作者：

Gao, Xvbo ^{[1
]}

Dong, Xiangting ^{[1
]}

Wang, Jinxian ^{[1
]}

Fan, Lijia ^{[1
]}

Liu, Guixia ^{[1
]}

机构：

[1] School of Chemistry and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022, China

来源：

Kuei Suan Jen Hsueh Pao/ Journal of the Chinese Ceramic Society | 2009年 / 37卷 / 04期

关键词：

Yttrium aluminum garnet - Calcination - Fourier transform infrared spectroscopy - Scanning electron microscopy - Fibers - Spectrometry - Fabrication - Yttrium - Electrospinning - Aluminum - Differential thermal analysis - X ray diffraction;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Polyvinylpyrrolidone (PVP)/[Y(NO3)3+Al(NO3)3] composite fiber was prepared by electrospinning. Yttrium aluminum garnet (YAG) nanofibers were fabricated by calcination of the relevant composite nanofibers. PVP/[Y(NO3)3+Al(NO3)3] composite nanofibers and YAG nanofibers were analyzed by using X-ray diffraction spectrometry, scanning electron microscopy, thermogravi- metric-differential thermal analysis and Fourier transform infrared spectrometry. The results show that PVP/[Y(NO3)3+Al(NO3)3] composite nanofiber is amorphous in structure, and pure phase YAG nanofibers are obtained by calcination of the PVP/[Y(NO3)3+Al(NO3)3] composite fibers at 900C for 10 h. The surface of as-prepared composite fibers is smooth, and the diameter of the composite fibers is about 175 nm. The diameter of the prepared YAG nanofibers is about 75 nm, and the length is greater than 100 μm. The mass of the sample remains constant when the temperature is above 550C, and the total mass loss percentage is 90.4%. The possible formation mechanism of the YAG nanofibers was preliminarily discussed.

引用

页码：580 / 585