Microstructural evaluation of oxide layers in CaO-added Mg alloys

被引:17
作者
Lee, Taeg-Woo [1 ]
Kim, Hyung-Giun [2 ]
So, Myoung-Gi [1 ]
Lee, Jin-Kyu [3 ]
Kim, Shae K. [4 ]
Park, Woo-Jin [5 ]
Kim, Won-Yong [4 ]
Kim, Sangshik [6 ]
Lim, Sung-Hwan [1 ]
机构
[1] Department of Advanced Materials Science and Engineering, Kangwon National University, Chuncheon
[2] Gangwon Regional Division, Korea Institute of Industrial Technology, Gangneung
[3] Research and Development, EMK, Wonju
[4] Korea Institute of Industrial Technology, Incheon
[5] Research Institute of Industrial Science and Technology, Gangneung
[6] Department of Metallurgical and Materials Engineering, ReCAPT, Gyeongsang National University, Chinju
关键词
Metals and alloys; Microstructure; Oxidation; Surfaces and interfaces; TEM; Transmission electron microscopy;
D O I
10.1016/j.jallcom.2015.02.101
中图分类号
学科分类号
摘要
A transmission electron microscopy analysis was conducted on the oxide layers of Mg-5.5Al-0.25Mn (AM60) alloys with different levels of CaO content formed in a thermogravimetric analyzer (TGA) system at 450 °C for 7 h. It was found that the oxide layer in AM60 + CaO grew as a columnar structure and, resultantly, that the oxide layers had different thicknesses with different levels of CaO content. The columnar oxide grains that were formed on the Mg + CaO alloy grew on the [1 0 0]MgO, resulting in a more compact and thicker initial oxide layer compared to the normal oxide layer. The columnar growth of the oxide layer in AM60 + CaO formed due to the Ca, which dissolved from CaO. © 2015 Elsevier B.V.
引用
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页码:5 / 10
页数:5
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