[1] Institute of Inorganic Chemistry, University of Regensburg, Regensburg,93040, Germany
[2] ICSM, CEA, CNRS, ENSCM, Univ Montpellier, Marcoule,34199, France
[3] Institut Laue-Langevin, 6 rue Jules Horowitz, Grenoble, Cedex 9,38042, France
[4] ESRF, European Synchrotron Radiation Facility, Grenoble,3800, France
[5] Laboratory of Soft Matter Electron Microscopy, University of Bayreuth, Bayreuth,95440, Germany