Preparation and characterization of Nd3+:ZnO-B2O3- Al2O3-SiO2 transparent glass-ceramics

被引：0
|
作者：
Zou, Xiang-Yu [1 ]
Zhang, Hong-Bo [1 ]
Su, Chun-Hui [1 ]
机构：
[1] College of Chemical and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022, China
来源：
Rengong Jingti Xuebao/Journal of Synthetic Crystals | 2012年 / 41卷 / 05期
关键词：
Avrami parameter - Crystallization activation energy - Fluorescence spectra - Kissinger equation - Melting and crystallization - Nucleating agents - Transparent glass ceramics - UV-VIS-NIR spectrophotometers - XRD - ZnO-B<inf>2</inf>O<inf>3</inf>- Al<inf>2</inf>O<inf>3</inf>-SiO<inf>2</inf>;
D O I：
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中图分类号：
学科分类号：
摘要：
Nd3+:ZnO-B2O3- Al2O3-SiO2 transparent glass-ceramic was prepared by melting and crystallization technology. The nucleating agent content on Nd3+:ZnO-B2O3- Al2O3-SiO2 transparent glass ceramic nucleation and crystallization performance were investigated by DTA, XRD, SEM, UV-Vis-NIR spectrophotometer, fluorescence spectrum measurement. The modified Kissinger equation of nucleating agent on the crystallization kinetics parameters, the crystallization activation energy E and crystallization kinetics of criterion, using Augis-Bennett equation to calculate Avrami parameter. the relations of microstructure and optical transmittance was analyzed, and the optical properties were studied.
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页码：1200 / 1204
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