Effect of brazing temperature on interfacial microstructure and properties of Ti60/Si3N4 brazed joints

被引:0
作者
Hu T. [1 ,2 ]
Lei Y. [2 ]
Hu S. [2 ]
Song X. [1 ]
Wang C. [2 ]
机构
[1] Harbin Institute of Technology, State Key Laboratory of Advanced Welding and Joining, Harbin
[2] Harbin Institute of Technology at Weihai, Shandong Provincial Key Laboratory of Special Welding Technology, Weihai
来源
Hanjie Xuebao/Transactions of the China Welding Institution | 2018年 / 39卷 / 08期
关键词
Brazing temperature; High-temperature titanium alloy; Silicon nitride ceramic;
D O I
10.12073/j.hjxb.2018390195
中图分类号
学科分类号
摘要
In order to study the effect of brazing temperature on the microstructure and mechanical properties of Ti60/Si3N4 joints, Ag-28Cu eutectic alloy was used to braze Ti60 alloy and Si3N4 ceramic at the temperature range from 870℃ to 910℃ for 10 min. The microstructure of the brazed joint was analyzed by Scanning Electron Microscope and Energy Dispersive Spectrometer. The typical interfacial microstructure was Ti60/Ti-Cu intermetallic layer/Ag(s,s)+Cu(s,s)/Ti-Cu intermetallic layer/Ti5Si3+TiN/Si3N4. The evolution process of the brazed joint was analyzed. The results showed that the thickness of Ti-Cu intermetallic layer next to Ti60 alloy and the Ti5Si3+TiN layer on Si3N4 ceramic side increased gradually with the increasing of brazing temperature. Meanwhile, the content of Ag(s,s) and Cu(s,s) decreased. In addition, Ti-Cu compound was formed in Ti5Si3+TiN layer by the reaction between element Ti which diffused to Si3N4 ceramic side and element Cu in the liquid phase. The shear test indicated that the highest shear strength of 61.7 MPa was obtained with the brazing technological parameter of 880℃+10 min. © 2018, Editorial Board of Transactions of the China Welding Institution, Magazine Agency Welding. All right reserved.
引用
收藏
页码:28 / 31and37
页数:3109
相关论文
共 6 条
[1]  
Wei S., Shi W., Wang D., Et al., Microstructure and mechanical properties of high temperature titanium alloy Ti60 at 600℃, The Chinese Journal of Nonferrous Metals, 20, 1, pp. s801-s806, (2010)
[2]  
Zhai H., Li J., Wu J., Et al., Applications and performance testing of high-temperature ceramics for heat engine components, Journal of Materials Engineering, 6, pp. 78-83, (2010)
[3]  
Lu H., Kang Z., Chu J., Et al., Microstructure and strength of SiC/Nb joint with Cu based brazing filler metal, Transactions of the China Welding Institution, 26, 1, pp. 29-31, (2005)
[4]  
He Y.M., Zhang J., Lu P.L., Et al., Characterization of the Si<sub>3</sub>N<sub>4</sub>/42CrMo joints vacuum brazed with Pd modified filler alloy for high temperature application, Vacuum, 109, pp. 86-93, (2014)
[5]  
Song X., Cao J., Lin X., Et al., Interfacial structure and properties of Si<sub>3</sub>N<sub>4</sub>/AgCu/TiAl brazing joints, Rare Metal Materials and Engineering, 40, 1, pp. 48-51, (2011)
[6]  
Zhao Y.X., Wang M.R., Cao J., Et al., Brazing TC4 alloy to Si<sub>3</sub>N<sub>4</sub> ceramic using nano-Si<sub>3</sub>N<sub>4</sub> reinforced AgCu composite filler, Materials & Design, 76, pp. 40-46, (2015)