Alumina thin film coated ammonium dinitramide fabricated by atomic layer deposition

被引:0
|
作者
Gong, Ting [1 ,2 ]
Qin, Li-Jun [1 ,2 ]
Yan, Rui [2 ]
Hu, Lan [2 ]
Ji, Yue-Ping [2 ]
Feng, Hao [1 ]
机构
[1] Laboratory of Material Surface Engineering and Nanofabrication, Xi'an Modern Chemistry Research Institute, Xi'an
[2] Science and Technology on Combustion and Explosion Laboratory, Xi'an Modern Chemistry Research Institute, Xi'an
来源
Wuji Cailiao Xuebao/Journal of Inorganic Materials | 2014年 / 29卷 / 08期
基金
中国国家自然科学基金;
关键词
Alumina; Ammonium dinitramide; Atomic layer deposition; Hygroscopicity;
D O I
10.15541/jim20130572
中图分类号
学科分类号
摘要
To deposit alumina thin films on ammonium dinitramide (ADN) by atomic layer deposition (ALD), trimethylaluminum and water were used as the precursors. The surface morphology and chemical compositions of the ALD alumina coated ADN were characterized by scanning electron microscope (SEM) and X-ray photoelectron spectroscope (XPS). The hygroscopic property of the ALD alumina coated ADN was studied by a vapor adsorption analyzer (VSA). The possible mechanism of ALD alumina film growth on the surface of ADN was discussed. The characterization results indicate that the ALD alumina film completely covers the surface of ADN. The thickness of the alumina film can reach hundreds of nanometers. After 48 h of air exposure, the shapes and topologies of the alumina coated ADN particles are maintained. The hygroscopicity of the ADN samples coated by 200 and 400 cycles of ALD alumina are 40.99% and 40.75%, respectively. Although the ALD alumina coating completely covers the surface of ADN and successfully maintains the shapes and topologies of ADN particles in a wet environment, the hygroscopicity of the ALD alumina coated ADN is not improved.
引用
收藏
页码:869 / 874
页数:5
相关论文
共 24 条
  • [1] Li S.W., Zhao F.Q., Yuan C., Et al., Tendency of research and development for overseas solid propellant, Journal of Solid Rocket Technology, 25, 2, pp. 36-42, (2002)
  • [2] Yang Q.J., Combustion characteristics and mechanisms of ammonium dinitramide, Journal of Propulsion Technology, 24, 2, pp. 97-103, (2003)
  • [3] Yue P., Heng S.Y., Han F., Et al., Compatibilities of ADN with five kinds of binders, Chinese Journal of Energetic Materials, 16, 1, pp. 66-69, (2008)
  • [4] Ma Y., Zhang H.L., Study on prilled ammonium dinitramide (ADN), Journal of Solid Rocket Technology, 25, 1, pp. 29-32, (2002)
  • [5] Xu H.X., Chen Z.Q., Zhao F.Q., Et al., Characteristic of prilled ammonium dinitramide photolyzed with sunlight, Chinese Journal of Energetic Materials, 15, 1, pp. 50-59, (2007)
  • [6] Xu H.X., Liao L.Q., Liu Q., Et al., Properties of prilled ammonium dinitramide (ADN) coated by polyurethane binders, Chinese Journal of Energetic Materials, 16, 6, pp. 712-715
  • [7] Zhang Z.Z., Ji Y.P., Wang B.Z., Et al., Application of ammonium dinitramide in propellants and explosives, Chinese Journal of Explosives and Propellants, 27, 3, pp. 36-41, (2004)
  • [8] Liu Q., Wang B.Z., Zhang H.H., Et al., Inorganic synthesis of ADN and its separation and purification, Chinese Journal of Energetic Materials, 14, 5, pp. 358-360, (2006)
  • [9] He J.X., Yang T.H., Zhang H.L., Et al., Synthesis and properties test of a new energetic compound guanidine dinitramide, Journal of Solid Rocket Technology, 24, 4, pp. 53-55, (2001)
  • [10] Thomas H., Heike P., Jasmin A., Et al., Ammonium dinitramide (ADN)-prilling, coating, and characterization, Propellants, Explosives, Pyrotechnics, 34, 3, pp. 231-238, (2009)