Investigation of Microstructure and Chemical Stability in Composites of NiAl Reinforced by Alumina-Silica Fibers

被引:0
作者
Gottstein, Günter [1 ]
Hu, Weiping [1 ]
机构
[1] Institut für Metallkunde und Metallphysik, RWTH, Aachen, Germany
关键词
Alumina-silica fibers - Complex thermodynamics - Composite specimens - Hot pressing temperature - In-vacuum - Interface structures - Ni diffusion - NiAl matrix - Sumitomo - Thermodynamic process;
D O I
10.3139/ijmr-2001-0213
中图分类号
学科分类号
摘要
Interface structure and chemical stability in composites of NiAl reinforced with alumina silica fibers (Sumitomo) were investigated by means of TEM, XEDS, EELS and electron diffraction. The composite specimens were fabricated by diffusion bonding in vacuum at 1300 ~ 1450 °C/ 5 ~ 15MPa/2h. The experimental results showed no Ni diffusion from the NiAl matrix into the fiber to occur during diffusion bonding. However, the fiber underwent complex thermodynamic processes depending on hot-pressing temperatures. They involved intrinsic chemical reactions between the fiber components to produce mullite and reduce silica, as well as extrinsic reactions between free oxygen and NiAl at the interface to generate α-Al2O3. The experimental results are discussed. © 2001 Carl Hanser Verlag, München.
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页码:1170 / 1174
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