Preparation of spherical activated carbon from alkali lignin

被引：0

作者：

College of Material Science and Engineering, Northeast Forestry University, Harbin, China ^{[1
]}

机构：

[1] College of Material Science and Engineering, Northeast Forestry University, Harbin

来源：

Chem. Ind. For. Prod. | / 1卷 / 16-22期

关键词：

Activate; Activated carbon; Spherical; Straw alkali lignin;

D O I：

10.3969/j.issn.0253-2417.2015.01.003

中图分类号：

学科分类号：

摘要：

Spherical activated carbon was prepared from the industrial alkali lignin via three steps: preparation of spherical lignin precursor, carbonization, and activation. Effects of preparation and activitation conditions of spherical lignin precursor on its morphology and particle size of the spherical activated carbon were investigated. SEM, N2(77K) adsorption-desorption isotherm, and FT-IR were used for characterizing its morphology structure, adsorption property, and surface functional groups, respectively. The results showed that spherical lignin precursor with diameter of approximate 5 μm could be obtained under the reaction temperature 90℃, stirring rate 200 r/min, reaction time 10 h, and pH 3.0. After carbonization at 300℃ followed by activation at 850℃, spherical activated carbon with BET surface area of 776.96 m2/g, total pore volume of 0.487 1 cm3/g, and average pore diameter of 2.51 mm could be obtained. ©, 2015, Editorial Board of Chemistry and Industry of Forest Products. All right reserved.

引用

页码：16 / 22

页数：6

共 15 条

[11] Zheng F.-E., Liu M.-H., Huang J.-Y., Et al., Adsorption behavious of L-aspartic acid on a spherical lignin adsorbent, Ion Exchange and Adsorption, 23, 5, pp. 400-407, (2007)
[12] Li X.-F., Luo X.-G., Preparation of characterization of spherical porous lignin particles, Journal of Functional Materials, 42, 2, pp. 256-263, (2011)
[13] Wang J.-T., Liu X.-J., Li Z.-S., Et al., Study on adsorption capability of pitch-based spherical activated carbon for endogenous glucose, Ion Exchange and Adsorption, 27, 3, pp. 247-256, (2011)
[14] Wang Z.-N., Zhan L., Ge M., Et al., Pith based spherical activated carbon for CO<sub>2</sub> removal from flue gases, Chemical Engineering Science, 66, 22, pp. 5504-5511, (2011)
[15] Liu C.-J., Liang X.-Y., Liu X.-J., Et al., Wettability modification of pitch-based spherical activated carbon by air oxidation and its effects on phenol adsorption, Applied Surface Science, 254, 9, pp. 2659-2665, (2008)

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