Synthesis of nanoflakes MoS2 by solid state hybrid microwave heating

被引：0

作者：

Xie, Mian-Yu ^{[1
,2
]}

Chen, Bing ^{[1
,2
]}

Yue, Song ^{[1
,2
]}

机构：

[1] Department of Physics, Jinan University, Guangzhou, China

[2] Siyuan Laboratory, Jinan University, Guangzhou, China

来源：

Rengong Jingti Xuebao/Journal of Synthetic Crystals | 2015年 / 44卷 / 05期

关键词：

High resolution transmission electron microscopy - Microwave heating - Molybdenum disulfide - Particle size - Layered semiconductors - Hybrid materials - X ray powder diffraction - Energy dispersive spectroscopy - Powders;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Molybdenum disulfide nano-powders were prepared by solid state hybrid microwave heating using Mo and S powders as starting materials within 45 minutes. The analysis by powder X-ray diffraction, energy dispersive X-ray spectroscopy, scanning electron microscopy and high resolution transmission electron microscopy reveal that the as-synthesized products are of single-phase hexagonal structure with the final compositions close to those of the starting materials. The results indicate that increasing the reacting temperature can optimize the product crystallization, decrease the particle size and promote the homogeneity. ©, 2015, Chinese Ceramic Society. All right reserved.

引用

页码：1394 / 1397