Assessment of x-ray micro-CT measurements of porosity and solute concentration distributions during diffusion in porous geologic media

被引:0
作者
机构
[1] Department of Earth Sciences, University of New Brunswick, Fredericton, NB
[2] Laboratory for Threat Material Detection, Department of Mechanical Engineering, University of New Brunswick, Fredericton, NB
关键词
Computed tomography; Diffusion; Porosity; Quantitative measurements; Tracer concentration;
D O I
10.1615/JPorMedia.v16.i8.10
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摘要
Using x-ray micro-computed tomography (micro-CT) for quantitative measurements in porous media is inherently challenged by uncertainties, which need to be identified and quantified to enable meaningful interpretation of measurements. For this purpose, we present results of experiments using micro-CT to measure the three-dimensional distribution of diffusion-accessible porosity and time-variant iodide tracer concentration within dolostone and sandstone samples. The precision, detection limits and spatial resolution of measurements were determined. Using a 0.6 M iodide tracer, the precision of attenuation coefficient measurement was approximately ±4%, in both the dolostone and sandstone samples. The precision for diffusion-accessible porosity and solute concentration measurements were ±7% and ±0.04 M, with detection limits of 20% and 0.12 M, respectively. The spatial resolution of measurement was 40 μm, representing the minimum size of features that can be distinctively resolved in a reconstructed image with 18.23 μm voxel size. © 2013 by Begell House, Inc.
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页码:683 / 694
页数:11
相关论文
共 25 条
  • [1] Benning J.L., Barnes D.L., The effects of scale and spatial heterogeneities on diffusion in volcanic breccias and basalts: Amchitka Island, Alaska, J. Contam. Hydrol., 106, pp. 150-165, (2009)
  • [2] Clausnitzer V., Hopmans J.W., Pore-scale measurements of solute breakthrough using microfocus x-ray computed tomography, Water Resour. Res., 36, pp. 2067-2079, (2000)
  • [3] Desplentere F., Lomov S.V., Woerdeman D.L., Verpoest I., Wevers M., Bogdanovich A., Micro-CT characterization of variability in 3D textile architecture, Compos. Sci. Technol., 65, pp. 1920-1930, (2005)
  • [4] Emerson D.W., Notes on mass properties of rocks: Density, porosity, permeability, Explor. Geophys., 21, pp. 209-216, (1990)
  • [5] Goldman L.W., Principles of CT: Radiation dose and image quality, J. Nucl. Med. Technol., 35, pp. 213-225, (2007)
  • [6] Huang T.T.Y., Jones A.S., He L.H., Darendeliler M.A., Swain M.V., Characterisation of enamel white spot lesions using x-ray micro-tomography, J. Dent., 35, pp. 737-743, (2007)
  • [7] Huber F., Enzmann F., Wenka A., Bouby M., Dentz M., Schafer T., Natural micro-scale heterogeneity induced solute and nanoparticle retardation in fractured crystalline rock, J. Contam. Hydrol., 133, pp. 40-52, (2012)
  • [8] Hussein E.M.A., Handbook on Radiation Probing, Gauging, Imaging and Analysis: Basics and Techniques, (2003)
  • [9] Hussein E.M.A., Computed Radiation Imaging: Physics and Mathematics of Forward and Inverse Problems, (2011)
  • [10] Hussein E.M.A., The physical and mathematical aspects of inverse problems in radiation detection and applications, Appl. Radiat. Isot., 70, pp. 1131-1135, (2012)