Detection of the elements Mn and Ni in a steel sample by laser-induced breakdown spectroscopy

被引:0
作者
Chen, Jin-Zhong [1 ]
Ma, Rui-Ling [1 ]
Wang, Jing [1 ]
Li, Xu [1 ]
Wang, Yin [1 ]
机构
[1] College of Physics Science and Technology, Hebei University, Baoding, 071002, Hebei
来源
Guangzi Xuebao/Acta Photonica Sinica | 2014年 / 43卷 / 12期
关键词
Laser-induced spectroscopy; Plane mirror device; Plasma; Quantitative analysis; Self-absorption effect; Spectroscopy; Standard steel sample;
D O I
10.3788/gzxb20144312.1214001
中图分类号
学科分类号
摘要
To reduce the influence of self-absorption of laser plasma emission spectra and improve the detection capability of laser-induced breakdown spectroscopy to material component, a plane mirror device was used to constraint the laser plasma. The spectral line profile of Mn and Ni in steel samples under different experimental condition were studied and analyzed quantitatively. The experimental results demonstrate that the self-absorption of spectral line decreases obviously when a plane mirror device is used. Through quantitatively analyzing Mn and Ni, once inserting a plane mirror device, the value of relative standard deviation of Mn decreases from 3.70% to 1.86%, and that of Ni decreases from 6.23% to 2.16%, which indicates that the measurements precision is improved obviously. It is thus clear that the plane mirror device could reduce the adverse effect of self-absorption on analyzing results obviously. ©, 2014, Chinese Optical Society. All right reserved.
引用
收藏
页数:5
相关论文
共 15 条
[1]  
Sarkar A., Alamelu D., Aggarwal S.K., Gallium quantification in solution by LIBS in the presence of bulk uranium, Optics and Laser Technology, 1, 44, pp. 30-34, (2012)
[2]  
Ermalitskaia F.E., Voropay Y.S., Zajogin A.P., Dual-pulse laser-induced breakdown spectrometry of bronze alloys and coatings, Journal of Applied Spectroscopy, 77, 2, pp. 153-159, (2012)
[3]  
Gondal M.A., Dastageer A., Maslehuddin M., Et al., Detection of sulfur in the reinforced concrete structures using a dual pulsed LIBS system, Optics and Laser Technology, 3, 44, pp. 566-571, (2012)
[4]  
Martelli M.R., Brygo F., Sadoudi A., Et al., Laser-Induced breakdown spectroscopy and chemometrics: a novel potential method to analyze wheat grains, Journal of Agricultural and Food Chemistry, 58, 12, pp. 7126-7134, (2010)
[5]  
Haiderr A.F., Khan Z.H., Determination of Ca content of coral skeleton by analyte additive method using the LIBS technique, Optics & Laser Technology, 6, 44, pp. 1654-1659, (2012)
[6]  
Leme F.O., Godoi Q., Kiyataka P.H., Et al., Effect of pulse repetition rate and number of pulses in the analysis of polypropylene and high density polyethylene by nanosecond infrared laser induced breakdown spectroscopy, Applied Surface Science, 8, 258, pp. 3598-3603, (2012)
[7]  
Peng L.L., Sun D.X., Su M.G., Et al., Rapid analysis on the heavy metal content of spent zinc-manganese batteries by laser-induced breakdown spectroscopy, Optics & Laser Technology, 8, 44, pp. 2469-2475, (2012)
[8]  
Elsayed K., Imam H., Harfoosh A., Et al., Design and construction of Q-switched Nd: YAG laser system for LIBS measurements, Optics and Laser Technology, 1, 44, pp. 130-135, (2012)
[9]  
Liu J., Gao X., Duan H.-H., Et al., Latest development of laser induced breakdown spectroscopy, Laser Journal, 33, 1, pp. 7-10, (2012)
[10]  
Sabsabi M., Cielo P., Quantitative analysis of aluminum alloys by laser-induced breakdown spectroscopy and plasma characterization, Applied Spectroscopy, 49, 4, pp. 499-507, (1995)