Synthesis and X-ray crystal structure of two novel ester ferrocenophanes

被引：0
作者：
Department of Chemistry, Northwest University, Xi'an, Shaanxi 710069, China [1 ]
机构：
[1] Department of Chemistry, Northwest University, Xi'an
来源：
Z. Naturforsch. Sect. B J. Chem. Sci. | 2007年 / 4卷 / 605-609期
关键词：
Ester ferrocenophanes; Hydrogen bonds; Synthesis; X-ray crystal structure;
D O I：
10.1515/znb-2007-0421
中图分类号：
学科分类号：
摘要：
Two novel ester ferrocenophanes have been prepared by esterification of 1,1′-ferrocenedi(carbonyl chloride) with glycol and 1,4-butanediol, respectively. Both of them have been characterized by IR, elemental analysis, MALDI-TOF MS and 1H NMR spectroscopic methods, and their structures have been elucidated by X-ray diffraction. The intermolecular associations based on C - H⋯O hydrogen bonds have also been discussed. These molecules are assembled into chains, and the chains are further assembled into a 3D structure through several hydrogen bonds. © 2007 Verlag der Zeitschrift für Naturforschung.
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页码：605 / 609
页数：4
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