Indirect electrochemical synthesis of nicotinic acid from nicotine

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作者：
Lu, Xu
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Jingxi Huagong/Fine Chemicals | 2000年 / 17卷 / 08期
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摘要：
Electro-oxidation of Cr2(SO4)3 on Pb/PbO2 anode in H2SO4 solution was carried out in a divided cell separated by an anion-exchange membrane. The influences of various factors such as concentration, current density, temperature, etc, were investigated. Under typical conditions appreciated, the average anodic current efficiency could reach 80%. Oxidation of nicotine with Cr2O72- was also studied. Results showed that the process employed gave higher yield, better product quality and less pollution.
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页码：453 / 455
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