A miniature X-ray diffraction setup on ID20 at the European Synchrotron Radiation Facility

被引：0

作者：

Sahle, Christoph J. ^{[1
]}

Majkut, Marta ^{[1
]}

Ruotsalainen, Kari O. ^{[1
]}

Gerbon, Florent ^{[1
]}

Suomalainen, Noora ^{[2
,3
]}

Lagier, Marie-Claire ^{[1
]}

Detlefs, Blanka ^{[1
]}

Claustre, Laurent ^{[1
]}

Mirone, Alessandro ^{[1
]}

Longo, Alessandro ^{[1
,4
]}

机构：

[1] ESRF European Synchrotron, 71 Ave Martyrs, F-38043 Grenoble 9, France

[2] Univ Helsinki, Dept Phys, POB 64, Helsinki 00014, Finland

[3] Univ Helsinki, Helsinki Inst Phys, Helsinki 00014, Finland

[4] UOS Palermo, Ist Studio Mat Nanostrutturati ISMN CNR, Via Ugo La Malfa 153, I-90146 Palermo, Italy

来源：

JOURNAL OF SYNCHROTRON RADIATION | 2024年 / 31卷

关键词：

X-ray diffraction; inelastic X-ray scattering; sample characterization; radiation damage; RAMAN-SCATTERING; SMALL-ANGLE; SPECTROMETER; DETECTOR;

D O I：

10.1107/S1600577524009147

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

We describe an ultra-compact setup for in situ X-ray diffraction on the inelastic X-ray scattering beamline ID20 at the European Synchrotron Radiation Facility. The main motivation for the design and construction of this setup is the increasing demand for on-the-fly sample characterization, as well as ease of navigation through a sample's phase diagram, for example subjected to high-pressure and/or high-temperature conditions. We provide technical details and demonstrate the performance of the setup.

引用

页码：1622 / 1626

页数：5

共 32 条

[1]

[Anonymous], 1963, XRAY DIFFRACTION CRY

[2] The fast azimuthal integration Python']Python library: pyFAI [J].

Ashiotis, Giannis ;

Deschildre, Aurore ;

Nawaz, Zubair ;

Wright, Jonathan P. ;

Karkoulis, Dimitrios ;

Picca, Frederic Emmanuel ;

Kieffer, Jerome .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2015, 48 :510-519

[3] Reduction of two-dimensional small- and wideangle X-ray scattering data [J].

Boesecke, Peter .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2007, 40 :S423-S427

[4] Tetracarbonates in silicate melts may be at the origin of a deep carbon reservoir in the deep Earth [J].

Cerantola, Valerio ;

Sahle, Christoph J. ;

Petitgirard, Sylvain ;

Wu, Min ;

Checchia, Stefano ;

Weis, Christopher ;

Di Michiel, Marco ;

Vaughan, Gavin B. M. ;

Collings, Ines E. ;

Arato, Robert ;

Wilke, Max ;

Jones, Adrian P. ;

Hanfland, Michael ;

Tse, John S. .

COMMUNICATIONS EARTH & ENVIRONMENT, 2023, 4 (01)

[5] Metal-support interaction and redox behavior of Pt(1 wt %)/Ce0.6Zr0.4O2 [J].

Deganello, G ;

Giannici, F ;

Martorana, A ;

Pantaleo, G ;

Prestianni, A ;

Balerna, A ;

Liotta, LF ;

Longo, A .

JOURNAL OF PHYSICAL CHEMISTRY B, 2006, 110 (17) :8731-8739

[6] PILATUS:: a two-dimensional X-ray detector for macromolecular crystallography [J].

Eikenberry, EF ;

Brönnimann, C ;

Hülsen, G ;

Toyokawa, H ;

Horisberger, R ;

Schmitt, B ;

Schulze-Briese, C ;

Tomizaki, T .

NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2003, 501 (01) :260-266

[7] CRYSTAL-STRUCTURE AND COMPRESSION OF RUBY TO 46 KBAR [J].

FINGER, LW ;

HAZEN, RM .

JOURNAL OF APPLIED PHYSICS, 1978, 49 (12) :5823-5826

[8] MiniPIX Timepix3-a miniaturized radiation camera with onboard data processing for online characterization of wide-intensity mixed-radiation fields [J].

Granja, C. ;

Jakubek, J. ;

Soukup, P. ;

Jakubek, M. ;

Turecek, D. ;

Marek, L. ;

Oancea, C. ;

Gohl, S. ;

Bergmann, B. ;

Pospisil, S. ;

Malich, M. ;

Vuolo, M. ;

Owens, A. ;

Zach, V ;

Stursa, J. ;

Chvatil, D. ;

Olsansky, V ;

Rucinski, A. ;

Gajewski, J. ;

Stasica, P. ;

Vykydal, Z. ;

Solc, J. .

JOURNAL OF INSTRUMENTATION, 2022, 17 (03)

[9] Directional detection of charged particles and cosmic rays with the miniaturized radiation camera MiniPIX Timepix [J].

Granja, Carlos ;

Kudela, Karel ;

Jakubek, Jan ;

Krist, Pavel ;

Chvatil, David ;

Stursa, Jan ;

Polansky, Stepan .

NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2018, 911 :142-152

[10] Two-dimensional detector software: From real detector to idealised image or two-theta scan [J].

Hammersley, AP ;

Svensson, SO ;

Hanfland, M ;

Fitch, AN ;

Hausermann, D .

HIGH PRESSURE RESEARCH, 1996, 14 (4-6) :235-248

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