Preparation of PZT(95/5) antiferroelectric nanoscale powders using sol-gel method

被引：0
|
作者：
Yao, Hai-Yun [1 ]
Hu, Yan-Hua [1 ]
Yu, Zhan-Jun [1 ]
Wang, Li-Xia [2 ]
机构：
[1] Department of Materials, Inner Mongolia University of Technology, Hohhot, China
[2] Technology Department of Fucheng Forging Company, Inner Mongolia First Machinery Manufacturing, Baotou, China
来源：
Gongneng Cailiao/Journal of Functional Materials | 2014年 / 45卷
关键词：
Sol-gel process - Differential thermal analysis - Powders - Nanotechnology - Perovskite;
D O I：
10.3969/j.issn.1001-9731.2014.Suppl.(2).030
中图分类号：
学科分类号：
摘要：
PZT(95/5) antiferroelectric nanoscale powders were prepared by sol-gel process. 550-750, calcination temperature range of dried PZT(95/5) powder were identified by differential thermal analysis. Dried powders were calcinated at 550, 600, 650, 750, holding for 2 hours, respectively. XRD analysis showed that the strength of the main crystalline phase gradually increases, the impurity phase peak height decreases with the increasing of the calcination temperature. When calcinated at 750, single perovskite phase was formed and PZT95/5 powders size was about 100 nm. ©, 2014, Journal of Functional Materials. All right reserved.
引用
收藏
页码：140 / 143
相关论文
共 50 条
  • [1] Preparation of PZT95/5 nano-powders with modified sol-gel method
    Xie, XH
    Dong, YM
    Yao, CH
    Qu, CF
    Dong, XL
    JOURNAL OF INORGANIC MATERIALS, 2004, 19 (01) : 81 - 85
  • [2] The preparation of PZT ultra-fine powders by sol-gel method and the dispersivity research
    Zhang, XG
    Liu, J
    Luo, Y
    Chen, C
    RARE METAL MATERIALS AND ENGINEERING, 2005, 34 : 194 - 197
  • [3] Preparation of PZT powders and ceramics via a hybrid method of sol-gel and ultrasonic atomization
    Xu, ZJ
    Chu, RQ
    Li, GR
    Shao, X
    Yin, QR
    MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY, 2005, 117 (02): : 113 - 118
  • [4] Preparation of superfine PZT powder by sol-gel method
    Xia, Dong-Lin
    Liu, Mei-Dong
    Zhou, Xue-Dong
    Zhao, Xiu-Jian
    Yadian Yu Shengguang/Piezoelectrics and Acoustooptics, 2005, 27 (03): : 331 - 334
  • [5] Photoluminescence of sol-gel synthesized PZT powders
    Rodriguez-Aranda, M. C.
    Calderon-Pinar, F.
    Hernandez-Landaverde, M. A.
    Heiras, J.
    Zamorano-Ulloa, R.
    Ramirez-Rosales, D.
    Yanez-Limon, J. M.
    JOURNAL OF LUMINESCENCE, 2016, 179 : 280 - 286
  • [6] Synthesis and Characterization of Nanocrystalline PZT Powders by a Simple Sol-Gel Method
    Zhang, Shaopeng
    Wang, Xiaohui
    Li, Longtu
    HIGH-PERFORMANCE CERAMICS VII, PTS 1 AND 2, 2012, 512-515 : 147 - 152
  • [7] Preparation of Al doped PZT thin films using a sol-gel method
    Iijima, T
    Sanada, N
    Hiyama, K
    Tsuboi, H
    Okada, M
    FERROELECTRIC THIN FILMS VIII, 2000, 596 : 223 - 228
  • [8] Seeding effects in the sol-gel preparation of lead zirconate titanate (PZT) powders
    Y. F. Chen
    R. Nass
    S. Vilminot
    Journal of Sol-Gel Science and Technology, 1997, 8 : 385 - 389
  • [9] Seeding effects in the sol-gel preparation of lead zirconate titanate (PZT) powders
    Chen, YF
    Nass, R
    Vilminot, S
    JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 1997, 8 (1-3) : 385 - 389
  • [10] Seeding Effects in the Sol-Gel Preparation of Lead Zirconate Titanate (PZT) Powders
    Y.F. Chen
    R. Nass
    S. Vilminot
    Journal of Sol-Gel Science and Technology, 1997, 8 : 385 - 389
12345