Controlled synthesis and characterisation of magnetite nanoparticles obtained by glycothermal method

被引：0
作者：
Bamoharram F.F. [1 ]
Hosseini K.D. [2 ]
Golmakani A. [1 ]
机构：
[1] Department of Chemistry, Islamic Azad University, Mashhad Branch, Mashhad
[2] Department of Chemistry, Khorasan Science and Technology Park (KSTP), Mashhad
来源：
International Journal of Nanomanufacturing | 2010年 / 5卷 / 3-4期
关键词：
Calcination; Glycothermal; Iron oxide; Magnetite; Nanoparticle; Temperature;
D O I：
10.1504/IJNM.2010.033866
中图分类号：
学科分类号：
摘要：
Iron oxide nanoparticles as Fe3O4, magnetite, were synthesised by the glycothermal reaction of metal acetylacetonate and 1,4-butanediol at 200-270°C. The products were then calcined at different temperatures in the range of 300-700°C. All products were characterised by TEM and XRD. It is found that the calcination temperature is an important factor and can control the product type. The nanoparticles were successfully synthesised with size ranges about 15 nm. Copyright © 2010 Inderscience Enterprises Ltd.
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页码：245 / 253
页数：8
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