Dynamic mechanical properties analysis of hollow gless microsphere reinforced epoxy resin composite

被引:0
作者
Wang C. [1 ,2 ]
Li H. [1 ]
Yu W. [1 ]
Wu J. [1 ]
Cui T. [1 ]
机构
[1] Key Laboratory of Mechanical Reliability for Heavy Equipments and Large Structures of Hebei Province, Yanshan University, Qinhuangdao
[2] Qinhuangdao Campus of Northeast Petroleum University, Qinhuangdao
来源
Fuhe Cailiao Xuebao/Acta Materiae Compositae Sinica | 2018年 / 35卷 / 05期
关键词
Dynamic mechanical temperature spectra; Epoxy resin; Hollow glass microsphere; Loss modulus; Master curves representing frequency dependence; Storage modulus; Time-temperature superposition;
D O I
10.13801/j.cnki.fhclxb.20170802.001
中图分类号
学科分类号
摘要
The dynamic mechanical analysis (DMA) for hollow for glass microsphere(HGM)/epoxy resin composite was conducted. The temperature-dependent mechanical properties were given for HGM/epoxy resin composite. The storage and loss moduli master curves for HGM/epoxy resin composite were presented through application of the time-temperature superposition on measurements at a series of temperatures. The influence of temperature, frequency, volume ratio and particle size on the storage and loss modalus was analyzed, and the influence mechanism was investigated by SEM for HGM/epoxy resin composite. It is found that the storage and loss moduli of the composite both increase as the HGM volume fraction is increased. The storage modulus decreases with the increasing temperature, the loss modulus initially increases significantly with temperature and then decreases, forming a peak near the glass transition temperature for HGM/epoxy resin composite. Ratio of less than 10% is good to improve its dynamic mechanical properties. The agglomeration of particles and the adhesion of the interface have great influence on the dynamic mechanical properties of HGM/epoxy resin composites. © 2018, Editorial Office of Acta Materiae Compositae Sinica. All right reserved.
引用
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页码:1105 / 1113
页数:8
相关论文
共 22 条
[1]  
Gong Y.M., Sun Z.J., Huo C.H., Et al., The dynamic viscoelastic properties of fiber reinforced epoxy resin composite materials under different preloading or dynamic loading, Acta Materiae Compositae Sinica, 23, 1, pp. 26-30, (2006)
[2]  
Zhou D.P., Xu P.H., Fan H., Viscoelastic characteristics of glass fiber reinforced phenolic materials-A storage modulus modeling methodology was developed, Journal of Materials Science and Engineering, 26, 6, pp. 963-965, (2008)
[3]  
Liang J.Z., Storage modulus and its characterization of inorganic particle filled polymer composites, Journal of South China University of Technology (Natural Science Edition), 36, 11, pp. 143-146, (2008)
[4]  
Jiang W.P., Zhu L.Y., Chen J., Et al., Study of carbon black/natural rubber composites by DMA, Journal of Elastomer, 25, 1, pp. 11-16, (2015)
[5]  
Qiao J., Amirkhizi A.V., Schaaf K., Et al., Dynamic mechanical analysis of fly ash filled polyurea elastomer, Journal of Engineering Materials and Technology, 133, 1, (2011)
[6]  
Zhang T.T., Han B.K., Zhang W.H., Et al., The dynamic modulus analysis of viscoelastic damping materials, Journal of Acoustics and Electronic Engineering, 4, pp. 46-48, (2011)
[7]  
Wang C.D., Zhang L.H., The WLF equation analysis in polymer physics, Journal of north China institute of technology, 25, 1, pp. 56-58, (2004)
[8]  
Lu Z.X., The research review of compound foam mechanical behavior, Journal of Mechanics, 34, 3, pp. 341-348, (2004)
[9]  
Plastinin A.V., Silvestrov V.V., The effect of strain rate on deformation and fracture of spheroplastic, Proceedings of 2nd ISIE'96, pp. 170-175, (1996)
[10]  
Kim H.S., Oh H.H., Manufacturing and impact behavior of syntactic foam, Journal of Applied Polymer Science, 76, 8, pp. 1324-1328, (2000)