Synthesis and Characterization of Novel Fluorine-containing Poly(aryl ether ketone)s

被引：0
|
作者：
Liu, Bai-Jun [1 ]
Chen, Chun-Hai [1 ]
Hu, Wei [1 ]
Sun, Hui [1 ]
Zhao, Shuang [1 ]
Jiang, Zhen-Hua [1 ]
Zhang, Wan-Jin [1 ]
Wu, Zhong-Wen [1 ]
机构：
[1] College of Chemistry, Jilin University, Changchun 130023, China
来源：
Kao Teng Hsueh Hsiao Hua Heush Hsueh Pao/ Chemical Journal of Chinese Universities | 2002年 / 23卷 / 02期
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摘要：
A kind of highly fluorinated bisphenol monomer was synthesized. It was characterized by FTIR, 1H NMR and MS. 6F-PEEK and 6F-PEEKK were prepared via aromatic nucleophilic substitution, based on [3,5-di(trifluoromethyl)] phenylhydroquinone and difluoro-monomers. The Tgs of 6F-PEEK and 6F-PEEKK are 423 and 436 K, respectively. The 6F-polymers exhibit a high thermal stability and good solubility. The flexible, creasable and transparent thin films were easily obtained by compression moulding and solution casting.
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