How to grow crystals for X-ray crystallography

被引：3
作者：
Sommer, Roger D. [1 ]
机构：
[1] Bristol Myers Squibb, 111 Squibb Dr North, New Brunswick, NJ 08902 USA
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 2024年 / 80卷
关键词：
crystal growth; X-ray crystallography; sublimation; vapor diffusion; mixed evaporation; layering; slow evaporation; slow cooling; solubility profile; CRYSTALLIZATION;
D O I：
10.1107/S2053229624006624
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Growing high-quality crystals remains a necessary part of crystallography and many other techniques. This article tabulates and describes several techniques and variations that will help individuals grow high-quality crystals in preparation for crystallographic techniques and other endeavors, such as form screening. The discussion is organized to focus on low-tech approaches available in any laboratory.
引用
收藏
页码：337 / 342
页数：6
相关论文
共 50 条
  • [41] Preparation of co-crystals of human PPARa-LBD and ligand for high-resolution X-ray crystallography
    Kamata, Shotaro
    Oyama, Takuji
    Ishii, Isao
    STAR PROTOCOLS, 2021, 2 (01):
  • [42] Counter-diffusion studies of human transthyretin: the growth of high-quality crystals for X-ray and neutron crystallography
    De'Ath, Clare
    Oliva, Mizar F.
    Moulin, Martine
    Blakeley, Matthew P.
    Haertlein, Michael
    Mitchell, Edward P.
    Gavira, Jose A.
    Bowler, Matthew W.
    Forsyth, V. Trevor
    JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2025, 58 : 107 - 118
  • [43] X-ray crystallography in Italy: from the early steps to the present days
    Viterbo, Davide
    RENDICONTI LINCEI-SCIENZE FISICHE E NATURALI, 2013, 24 : S19 - S32
  • [44] Direct methods and refinement in electron and X-ray crystallography - diketopiperazine revisited
    Dorset, Douglas L.
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-CRYSTALLINE MATERIALS, 2010, 225 (2-3): : 86 - 93
  • [45] Synthesis, X-Ray Crystallography and Leishmanicidal Activity of Benzimidazolinyl Piperidine derivative
    Saify, Zafar Saied
    Mallick, Tabinda Zarreen
    Begum, Nasreen
    Yousuf, Samar
    Saeed, Syed Muhammad Ghufran
    Haider, Shazia
    Ashraf, Seema
    Qaiser, Shama
    JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN, 2014, 36 (06): : 1145 - 1149
  • [46] Application of magnetically oriented microcrystal array to X-ray and neutron crystallography
    Tsukui, Shu
    Kimura, Fumiko
    Kimura, Tsunehisa
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2015, 71 : S274 - S275
  • [47] Protein production in Escherichia coli for structural studies by X-ray crystallography
    Goulding, CW
    Perry, LJ
    JOURNAL OF STRUCTURAL BIOLOGY, 2003, 142 (01) : 133 - 143
  • [48] Characterization of Glycoproteins with the Immunoglobulin Fold by X-Ray Crystallography and Biophysical Techniques
    Ereno-Orbea, June
    Sicard, Taylor
    Cui, Hong
    Akula, Indira
    Julien, Jean-Philippe
    JOVE-JOURNAL OF VISUALIZED EXPERIMENTS, 2018, (137):
  • [49] Multi-view Learning for Classification of X-Ray Crystallography Images
    Lekamge, B. M. Thamali
    Sowmya, Arcot
    Newman, Janet
    MACHINE LEARNING AND DATA MINING IN PATTERN RECOGNITION (MLDM 2016), 2016, 9729 : 446 - 458
  • [50] Uracil recognition in archaeal DNA polymerases captured by X-ray crystallography
    Firbank, Susan J.
    Wardle, Josephine
    Heslop, Pauline
    Lewis, Richard J.
    Connolly, Bernard A.
    JOURNAL OF MOLECULAR BIOLOGY, 2008, 381 (03) : 529 - 539
12345