How to grow crystals for X-ray crystallography

被引:3
作者
Sommer, Roger D. [1 ]
机构
[1] Bristol Myers Squibb, 111 Squibb Dr North, New Brunswick, NJ 08902 USA
来源
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 2024年 / 80卷
关键词
crystal growth; X-ray crystallography; sublimation; vapor diffusion; mixed evaporation; layering; slow evaporation; slow cooling; solubility profile; CRYSTALLIZATION;
D O I
10.1107/S2053229624006624
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Growing high-quality crystals remains a necessary part of crystallography and many other techniques. This article tabulates and describes several techniques and variations that will help individuals grow high-quality crystals in preparation for crystallographic techniques and other endeavors, such as form screening. The discussion is organized to focus on low-tech approaches available in any laboratory.
引用
收藏
页码:337 / 342
页数:6
相关论文
共 50 条
  • [31] Life in the fast lane for protein crystallization and X-ray crystallography
    Pusey, ML
    Liu, ZJ
    Tempel, W
    Praissman, J
    Lin, DW
    Wang, BC
    Gavira, JA
    Ng, JD
    PROGRESS IN BIOPHYSICS & MOLECULAR BIOLOGY, 2005, 88 (03) : 359 - 386
  • [32] Analysis of xenon binding to photosystem II by X-ray crystallography
    J. W. Murray
    K. Maghlaoui
    J. Kargul
    M. Sugiura
    J. Barber
    Photosynthesis Research, 2008, 98 : 523 - 527
  • [33] Novel organophosphorus compounds; synthesis, spectroscopy and X-ray crystallography
    Shariatinia, Zahra
    Sohrabi, Marzieh
    Yousefi, Mohammad
    Koval, Tomas
    Dusek, Michal
    MAIN GROUP CHEMISTRY, 2012, 11 (02) : 125 - 133
  • [34] X-ray crystallography and NMR spectroscopy of some cyclohexyl esters
    Baldwin, CR
    Britton, MM
    Davies, SC
    Gillies, DG
    Hughes, DL
    Smith, GW
    Sutcliffe, LH
    JOURNAL OF MOLECULAR STRUCTURE, 1997, 403 (1-2) : 1 - 16
  • [35] Applications of X-ray and Electron Crystallography in Structural Investigations of Zeolites
    Ma, Chao
    Liu, Xiaona
    Nie, Chenyang
    Chen, Lu
    Tian, Peng
    Xu, Hongyi
    Guo, Peng
    Liu, Zhongmin
    CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE, 2021, 42 (01): : 188 - 200
  • [36] PPARα-Ligand Binding Modes Revealed by X-ray Crystallography
    Kamata, Shotaro
    Ishii, Isao
    YAKUGAKU ZASSHI-JOURNAL OF THE PHARMACEUTICAL SOCIETY OF JAPAN, 2021, 141 (11): : 1267 - 1274
  • [37] Use of X-ray crystallography for the characterization of single crystals grown in steroid containing transdermal drug delivery systems
    Lipp, R
    Müller-Fahrnow, A
    EUROPEAN JOURNAL OF PHARMACEUTICS AND BIOPHARMACEUTICS, 1999, 47 (02) : 133 - 138
  • [38] Beamline X29: a novel undulator source for X-ray crystallography
    Shi, Wuxian
    Robinson, Howard
    Sullivan, Michael
    Abel, Don
    Toomey, John
    Berman, Lonny E.
    Lynch, Don
    Rosenbaum, Gerd
    Rakowsky, George
    Rock, Larry
    Nolan, Bill
    Shea-McCarthy, Grace
    Schneider, Dieter
    Johnson, Erik
    Sweet, Robert M.
    Chance, Mark R.
    JOURNAL OF SYNCHROTRON RADIATION, 2006, 13 : 365 - 372
  • [39] The use of X-ray Crystallography to Determine Absolute Configuration (II)
    Flack, Howard D.
    ACTA CHIMICA SLOVENICA, 2008, 55 (04) : 689 - 691
  • [40] X-ray Crystallography: Seeding Technique with Cytochrome P450 Reductase br
    Zhang, Bixia
    Lewis, Jacob A.
    Hazra, Rishi
    Kang, ChulHee
    BIO-PROTOCOL, 2022, 12 (21):