Solvothermal preparetion and near-infrared fluorescence of BaSnO3 nanoparticles

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作者
机构
[1] Xie, Li-Juan
[2] Cai, Jian-Liang
[3] Zhang, Rui
[4] Zou, Yang
[5] Meng, Jian-Xin
来源
Meng, J.-X. (tmjx@jnu.edu.cn) | 2013年 / Editorial Office of Chinese Optics卷 / 34期
关键词
Particle size - Synthesis (chemical) - Infrared devices - Emission spectroscopy - High resolution transmission electron microscopy - Calcination - Particle size analysis - Barium compounds - Fluorescence - Solid state reactions - Tin compounds - X ray diffraction;
D O I
10.3788/fgxb20133401.0018
中图分类号
学科分类号
摘要
BaSnO3 nano-phosphors were prepared by solvothermal method using glycol-water mixed solution as a solvent, followed by calcinations at different temperature. The as-synthesized samples were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), the nano-particle size analyzer, UV-Vis-NIR spectrophotometer, excitation and emission spectra. The nano-powders are sphere with sizes of 30~50 nm. Good dispersity can be achieved even after the sample was calcined. Efficient near-infrared fluorescence with emission peak of 895 nm was observed under the excitation of 385 nm. Comparing with the sample prepared by solid state reaction, the emission intensities increase about ten folds. The degree of crystallization is found to be the main fact of the near-infrared fluorescence of BaSnO3 nanoparticles.
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